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Spicy spice for kretek blasting bead, preparation method and application thereof

A technology of spicy essence and popping beads, which is applied in the direction of essential oil/fragrance, tobacco, application, etc., can solve the problems of affecting consumers' sensory experience and aggravating chemical smell, and achieves small incision, simple preparation method and good stability Effect

Inactive Publication Date: 2015-07-29
HUBEI CHINA TOBACCO IND +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the cracking process of cigarette beads, the wall material is destroyed and the solvent is released. During this process, the chemical smell is obviously aggravated, which seriously affects the sensory experience of consumers.

Method used

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  • Spicy spice for kretek blasting bead, preparation method and application thereof
  • Spicy spice for kretek blasting bead, preparation method and application thereof
  • Spicy spice for kretek blasting bead, preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] 1. Pretreatment of raw materials: Weigh the clove buds, wash them, dry them in the shade, then crush them, pass through a 100-150 mesh sieve, and set aside;

[0024] 2. Soaking: add 75% ethanol that is 25 times the weight of clove bud powder and soak for 24 hours;

[0025] 3. Ultrasonic extraction: Ultrasonic time is 60min, ultrasonic power is 40w, filter, and the filtrate is refluxed three times at 80°C for separation to obtain clove bud oil;

[0026] 4. Dilute the above thymol with propylene glycol to a 10% solution, shake well until completely dissolved, and set aside;

[0027] 5. Dilute the above-mentioned vanillin with propylene glycol to a 10% solution, shake well until completely dissolved, and set aside;

[0028] 6. The parts by weight are 3 parts of clove bud oil, 0.8 part of eugenol, 0.2 part of 10% thymol, 0.5 part of β-caryophyllene, 0.5 part of guaiacol, 1.0 part of isoeugenol, 10% pandan Mix 3 parts of benzyl alcohol, 0.7 part of benzyl alcohol and 90.3 ...

Embodiment 2

[0030] 1. Pretreatment of raw materials: Weigh the clove buds, wash them, dry them in the shade, then crush them, pass through a 100-150 mesh sieve, and set aside;

[0031] 2. Soaking: add 75% ethanol that is 25 times the weight of clove bud powder and soak for 36 hours;

[0032] 3. Ultrasonic extraction: Ultrasonic time is 60min, ultrasonic power is 40w, filter, and the filtrate is refluxed three times at 80°C for separation to obtain clove bud oil;

[0033] 4. Dilute the above thymol with propylene glycol to a 10% solution, shake well until completely dissolved, and set aside;

[0034] 5. Dilute the above-mentioned vanillin with propylene glycol to a 10% solution, shake well until completely dissolved, and set aside;

[0035] 6. The parts by weight are 2 parts of clove bud oil, 0.5 part of eugenol, 0.1 part of 10% thymol, 0.8 part of β-caryophyllene, 0.8 part of guaiacol, 0.5 part of isoeugenol, 10% pandan 1 part of benzyl alcohol, 0.5 part of benzyl alcohol and 93.8 parts...

Embodiment 3

[0037] 1. Pretreatment of raw materials: Weigh the clove buds, wash them, dry them in the shade, then crush them, pass through a 100-150 mesh sieve, and set aside;

[0038] 2. Soaking: add 75% ethanol that is 25 times the weight of clove bud powder and soak for 30 hours;

[0039] 3. Ultrasonic extraction: Ultrasonic time is 60min, ultrasonic power is 40w, filter, and the filtrate is refluxed three times at 80°C for separation to obtain clove bud oil;

[0040] 4. Dilute the above thymol with propylene glycol to a 10% solution, shake well until completely dissolved, and set aside;

[0041] 5. Dilute the above-mentioned vanillin with propylene glycol to a 10% solution, shake well until completely dissolved, and set aside;

[0042] 6. The parts by weight are 5 parts of clove bud oil, 1.0 part of eugenol, 0.3 part of 10% thymol, 0.2 part of β-caryophyllene, 0.2 part of guaiacol, 0.8 part of isoeugenol, and 10% pandan 5 parts of benzyl alcohol, 1.0 part of benzyl alcohol and 86.5 ...

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Abstract

The invention provides a spicy spice for a kretek blasting bead, a preparation method and application thereof. The spicy spice is characterized in that the spicy spice is prepared by mixing the following raw materials in percentage by weight: 2 to 5 percent of clove bud oil, 0.5 to 1 percent of eugenol, 0.01 to 0.03 percent of thymol, 0.2 to 0.8 percent of beta-caryophyllene, 0.2 to 0.8 percent of guaiacol, 0.5 to 1 percent of isoeugenol, 0.1 to 0.5 percent of vanillin, 0.5 to 1 percent of benzyl alcohol, and the balance of a solvent. The spicy spice can not only cover adverse chemical smell produced by wall materials and package solvent when the kretek blasting bead is pinched, but also provide spicy fragrance coordinated with the fragrance of the tobacco, makes up the situation of distortion of clove fragrance during burning of the kretek, and enables the kretek to have conformable and natural spicy fragrance.

Description

technical field [0001] The invention relates to the field of flavors and fragrances for tobacco, in particular to a spice flavor for clove cigarette popping beads, a preparation method and application thereof. Background technique [0002] With the continuous improvement of people's economic level and the change of the concept of cigarette consumption, spicy-flavored cigarettes are becoming more and more popular among smokers, such as clove cigarettes in Indonesia. Spicy flavors are mostly achieved through traditional shredded tobacco flavoring. Although traditional shredded tobacco flavoring can give cigarettes a spicy aroma, the shredded tobacco is burned and thermally cracked, resulting in distortion of the spicy aroma when smoking, which is not in harmony with the original aroma of tobacco, affecting the sensory experience. [0003] For this reason, existing a large amount of scientific research workers have carried out the research on the method of flavoring by popping...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/30
Inventor 祃志明熊国玺陈胜孙炜炜李星
Owner HUBEI CHINA TOBACCO IND
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