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Preparation method of briquetted active carbon

A technology of activated carbon and carbonization, applied in the field of coal chemical industry, can solve the problems of limited use range, inability to adjust pore structure, unstable performance, etc., and achieve significant economic benefits, improve economic benefits, and improve activation efficiency.

Active Publication Date: 2015-04-22
PINGLUO XIANGTAI COAL CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Anthracite plus tar formed columnar activated carbon, because the raw materials and products used are very different from briquetted activated carbon, and its cost is high, and the carbonization has a great impact on the environment
Raw smoke crushed carbon, this kind of activated carbon is low-grade activated carbon, low cost, and the product quality is due to the high floating rate and the pore structure cannot be adjusted, so its application range is limited, and the coal quality is strict.
[0004] The briquette activated carbon has low ash, good molding, good pore forming, and has certain adhesiveness, and the strength is above 90, but it has higher requirements for the production of raw coal
Strength is an important indicator of the performance of briquetted activated carbon. The cohesiveness of weakly caking coal is appropriate, and briquetted activated carbon with adsorption indicators that meet the requirements can be prepared, but the reserves of this weakly caking coal are very limited; although the coal reserves are relatively large. Low, the strength of the manufactured briquetted activated carbon products is difficult to meet the market demand
The raw coal for the production of briquetted activated carbon needs to be found in coking coal. However, due to the high ash content and poor washability of coking coal in my country, it is difficult to meet the production requirements of briquetted activated carbon. At present, the briquetted activated carbon products produced by the existing technology are still There are defects such as high production cost and unstable performance

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] (1) Oxidation and drying of coal:

[0033] Take by weighing long-flame coal 990Kg after washing, A d : 4%, V d : 36%. It is sent to the rotary dryer, and after mass transfer and heat transfer, it is discharged into the drying material scraper conveyor by the rotary dryer, and sent to the dry coal silo through the bucket elevator for standby. Drying is heated by carbonized coal gas, passes through the combustion furnace, and is equipped with air to adjust the temperature, enters the rotary drying furnace, contacts with raw coal in the furnace, and oxidizes and dries, and the exhaust gas after drying is discharged from the rotary dryer , and then discharged into the chimney through the fan. The gas temperature at the inlet of the dryer is ≯600°C, and the gas temperature at the outlet of the dryer is less than 90°C.

[0034] (2) Ingredients section:

[0035] Take the dried coal material of step (1), enter the scraper machine through the quantitative screw feeder, weigh...

Embodiment 2

[0054] (1) Oxidation and drying of coal:

[0055] Take by weighing the long-flame coal 950Kg after washing, A d : 4%, V d : 36%. It is sent to the rotary dryer, and after mass transfer and heat transfer, it is discharged into the drying material scraper conveyor by the rotary dryer, and sent to the dry coal silo through the bucket elevator for standby. Drying is heated by carbonized coal gas, passes through the combustion furnace, and is equipped with air to adjust the temperature, enters the rotary drying furnace, contacts with raw coal in the furnace, and oxidizes and dries, and the exhaust gas after drying is discharged from the rotary dryer , and then discharged into the chimney through the fan. The gas temperature at the inlet of the dryer is ≯600°C, and the gas temperature at the outlet of the dryer is less than 90°C.

[0056] (2) Ingredients section:

[0057] Take the dried coal material of step (1), enter the scraper machine through the quantitative screw feeder, w...

Embodiment 3

[0077] (1) Oxidation and drying of coal:

[0078] Weigh 900Kg of long-flame coal after washing, A d : 4%, V d : 36%. It is sent to the rotary dryer, and after mass transfer and heat transfer, it is discharged into the drying material scraper conveyor by the rotary dryer, and sent to the dry coal silo through the bucket elevator for standby. Drying is heated by carbonized coal gas, passes through the combustion furnace, and is equipped with air to adjust the temperature, enters the rotary drying furnace, contacts with raw coal in the furnace, and oxidizes and dries, and the exhaust gas after drying is discharged from the rotary dryer , and then discharged into the chimney through the fan. The gas temperature at the inlet of the dryer is ≯600°C, and the gas temperature at the outlet of the dryer is less than 90°C.

[0079] (2) Ingredients section:

[0080] Take the dried coal material of step (1), enter the scraper machine through the quantitative screw feeder, weigh 50Kg of...

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Abstract

The invention relates to a preparation method of briquetted active carbon, which sequentially comprises the following technical processes: (1) oxidizing and drying a coal material; (2) mixing; (3) pulverizing; (4) molding; (5) charring; (6) drying the charred material; (7) activating; (8) screening the activated material; (9) performing acid pickling; and (10) drying the acid-pickled material. The method has the advantages of low investment, high yield, favorable environmental protection effect, low cost and low comprehensive energy consumption. The product has the characteristics of light bulk specific gravity, well-developed macropores, mesopores and minipores, and high adsorption speed.

Description

technical field [0001] The invention belongs to the field of coal chemical industry, in particular to a method for preparing activated carbon, in particular to a method for preparing briquetted activated carbon. Background technique [0002] Activated carbon is a hydrophobic adsorbent made from carbon-containing substances as raw materials, which is carbonized and activated at high temperature. Activated carbon contains a large number of micropores, has a huge specific surface area, can effectively remove color, odor, and remove organic pollutants and some inorganic substances in water bodies. It is widely used in environmental protection, chemical industry and other fields. Therefore, its The demand is increasing year by year. my country has abundant coal reserves, which can be effectively used to prepare coal-based activated carbon. According to different raw materials, coal-based activated carbon is divided into crushed activated carbon, columnar activated carbon and br...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/10C01B32/336
Inventor 庄林生庄骏飞
Owner PINGLUO XIANGTAI COAL CHEM
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