Epoxidized styrene-isoprene-styrene block copolymer medical patch and preparation method thereof
A technology of epoxidizing styrene and styrene blocks, which is used in pharmaceutical formulations, medical preparations with non-active ingredients, and sheet transportation, etc., can solve the problems of easy occurrence of allergies, impact on sticking performance, poor adhesion ability, etc. , to avoid skin whitish allergy, improve the mixing amount of the drug, and enhance the adhesion performance.
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Embodiment 1
[0021] Example 1: Preparation of epoxidized styrene-isoprene-styrene block copolymer medical patch
[0022] raw material:
[0023]
[0024]
[0025] (1) Preparation method:
[0026] Part of naphthenic soybean oil was firstly added to the reaction kettle, ESIS and SEPS were added according to weight ratio, then antioxidant was added, heated to 160°C, stirring was started, and nitrogen was introduced to replace the gas in the kettle.
[0027] After the ESIS is completely dissolved, add the rosin pentaerythritol resin in proportion, and then add the hydrogenated rosin resin with a constant temperature.
[0028] The kettle was subjected to vacuum treatment to keep it at -0.02mPa, stirred for about 20min to lower the temperature of the kettle, and the temperature was lowered to 120°C by cooling in the reactor before discharging.
[0029] (2) Product performance parameters:
[0030] Appearance: with light yellow transparent solid glue
[0031] Non-volatile matter: 100%
...
Embodiment 2
[0039] Example 2: Preparation of epoxidized styrene-isoprene-styrene block copolymer medical patch
[0040] raw material:
[0041]
[0042]
[0043] (4) Preparation method:
[0044] Part of naphthenic soybean oil was firstly added to the reaction kettle, ESIS and SEPS were added according to weight ratio, then antioxidant was added, heated to 160°C, stirring was started, and nitrogen was introduced to replace the gas in the kettle.
[0045] After the ESIS is completely dissolved, add the rosin pentaerythritol resin in proportion, and then add the hydrogenated rosin resin with a constant temperature.
[0046] The kettle was subjected to vacuum treatment to keep it at -0.05mPa, stirred for about 20 minutes to lower the temperature of the kettle, and the temperature was lowered to 120°C by using the inner cooling of the reactor to discharge the material.
[0047] (5) Product performance parameters:
[0048] Appearance: with light yellow transparent solid glue
[0049] N...
Embodiment 3
[0057] Example 3: Preparation of epoxidized styrene-isoprene-styrene block copolymer medical patch
[0058] raw material:
[0059]
[0060]
[0061] (7) Preparation method:
[0062] Part of naphthenic soybean oil was firstly added to the reaction kettle, ESIS and SEPS were added according to weight ratio, then antioxidant was added, heated to 160°C, stirring was started, and nitrogen was introduced to replace the gas in the kettle.
[0063] After the ESIS is completely dissolved, add the rosin pentaerythritol resin in proportion, and then add the hydrogenated rosin resin with a constant temperature.
[0064] The kettle was subjected to vacuum treatment to keep it at -0.03mPa, stirred for about 20 minutes to lower the temperature of the kettle, and the temperature was lowered to 120°C by cooling in the reactor before discharging.
[0065] (8) Product performance parameters:
[0066] Appearance: with light yellow transparent solid glue
[0067] Non-volatile matter: 100...
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