Taste improver for high intensity sweetener
A technology of sweeteners and improvers, which can be used in food ingredients as taste improvers, food preparation, food science, etc., and can solve problems such as unpleasant aftertaste, food taste, and aroma changes
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manufacture example 1
[0065] [Production Example 1]
[0066]Add 100 kg of 99 volume % ethanol to 10 kg of dried flower heads of golden buttons (crushed into about 5 mm), and extract at 75° C. to reflux temperature for 5 hours. After the extract was cooled to 40° C., solid-liquid separation was carried out with a centrifuge, and the extract was concentrated to 20 kg under reduced pressure. Add 0.2 kg of activated carbon to the concentrated solution, stir for 1 hour, add diatomaceous earth and filter under pressure to remove the activated carbon, then concentrate under reduced pressure to obtain 0.43 kg of gold button concentrate. 2 kg of distilled water was added to the concentrate, and extracted three times with 2 kg of ethyl acetate. Combine the extracted ethyl acetate layers, add diatomaceous earth and filter under pressure, then concentrate under reduced pressure to obtain 0.31 kg of crude extract of golden button. The yield was 3.1%. In addition, the spilanthol content was 12.4% by mass. M...
manufacture example 2
[0067] [Manufacturing Example 2]
[0068] The dried flower heads of 300 g of golden buttons were reflux extracted with 3200 g of 95 volume % ethanol for 1 hour. After cooling the extract and separating the solid and liquid, add diatomaceous earth and filter. After distilling off ethanol from the filtrate by concentrating under reduced pressure, 300 g of water was added and extracted three times with 300 ml of hexane. The extracted hexane layers were combined, and the hexane was evaporated by concentration under reduced pressure to obtain 8.4 g of a crude extract. The yield was 2.8% (spilanthol content: 9.5% by mass). The 8.4g crude extract was separated by silica gel chromatography (silica gel 200g, Φ5cm) (eluted with n-hexane: ethyl acetate = 8: 2), and the spilanthol component was separated (Rf value = 0.2-0.3 n-hexane: ethyl acetate=7:3), and the solvent was distilled off under reduced pressure to obtain 2.76 g of crude spilanthol fraction 1. Next, the crude spilanthol...
manufacture example 3
[0069] [Manufacture Example 3]
[0070] After 500 g of green coffee beans were finely ground, 5000 ml of a 70% by volume ethanol aqueous solution was added thereto, followed by heating under reflux for 2 hours. After the solution was cooled, solid-liquid separation was performed with a centrifugal filter, the filtrate was concentrated under reduced pressure to an ethanol content of 5% by mass or less, and 1,000 units of chlorogenic esterase (manufactured by Kitskoman) was added to the solution. Stir at 40°C for 3 hours. After the insolubles were removed by centrifugation, the treated liquid was introduced into a column filled with 1000 ml of synthetic adsorbent (Mitsubishi Chemical Industry Co., Ltd. (Mitsubishi Chemical Industry) Co., Ltd. (Mitsubishi Chemical Industry) Co., Ltd. (Mitsubishi Chemical Industry) Co., Ltd. (Mitsubishi Chemical Industry Co., Ltd., Dai Yaion (registered trademark) HP-20)) column, and the eluted The solution was freeze-dried to obtain 26.6 g of a...
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