Lachnum melanin hair dye and preparation method thereof

A technology of Trichomyces granulosa and melanin, applied in the field of Trichomyces granulosa melanin hair dye and its preparation, can solve the problems of unstable chromophoric groups of natural dyes, unsatisfactory fastness of natural dyes, and incomplete chromatogram of natural dyes, etc. Achieve good light protection, bright dyeing effect, easy to use

Inactive Publication Date: 2012-09-26
HEFEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] According to "Journal of Hengyang Normal University" (2009, 30 (6): 85-88), existing natural hair dyes are much superior than chemical hair dyes in avoiding skin allergies and side effects; but natural hair dyes are also There are some problems: First, the stability of natural pigments is poor, mainly because natural pigments are easily affected by external factors such as pH value, light (especially ultraviolet light), temperature, etc., which will change the structure or composition of natural pigments , so that its color changes; the second is that natural dyes are directly deposited on the surface of the hair through their affinity with the hair, but they have not penetrated into the cortex. The fastness is not ideal; in addition, natural dyes are not only incomplete in color spectrum, but also relatively grayish in color, and the color yield is low. Dyeing the same color requires a higher concentration, and the dyeing time is too long
However, it has not been reported so far that a new hair dye can be developed by adding Trichomelanin melanin to the existing oxidative hair dye formula to reduce the content of p-phenylenediamine in the hair dye.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] First, according to the Chinese patent application number 200910145058.4 "A kind of Trichomyces granulosa and its method for preparing melanin by liquid fermentation", the extracellular melanin is prepared by using the Trichomyces granulosa YM-223 with the preservation number of CCTCC No: M 209193: Discobacteria YM-223 was inoculated in a 250mL Erlenmeyer flask filled with 125mL fermentation medium (PDA modified medium), and cultured at 25°C with constant temperature shaking at 200r / min for 10-15 days. After the cultivation, the supernatant was obtained by suction filtration, and the pH value of the obtained supernatant was adjusted to 10-11 with a NaOH aqueous solution with a concentration of 2 mol / L. Adjust the pH value to 2-3, let it stand overnight, centrifuge the resulting flocculent precipitate at 5,000r / min for 10 minutes, pour off the supernatant; add deionized water to the obtained solid precipitate and mix well Centrifuge at 5,000 r / min for 10 min, pour off th...

Embodiment 2

[0024] First, according to the Chinese patent application number 201110072469.2 "A strain of Trichodia singeri and its liquid fermentation method for preparing intracellular melanin", it was prepared by using a strain of Trichosanthes singeri YM-292 with a preservation number of CCTCC No: M 2011054 Intracellular melanin: inoculate Trichodia singerii YM-292 bacteria block into a 250mL Erlenmeyer flask filled with 50mL fermentation medium, and culture at 27°C with constant temperature shaking at 160r / min for 8-10 days. After the cultivation, the fermentation broth was centrifuged to obtain mycelia, and the mycelia was dried at 60° C. and ground, and the weight of mycelia (g): volume of NaOH solution (mL) = 1: 50-100 Liquid ratio Add the mycelium to the NaOH solution with a concentration of 1mol / L, extract it in a water bath at 80°C for 40 minutes, filter it with suction, adjust the pH value of the filtrate to 2-3 with 12mol / L hydrochloric acid, let it stand overnight, and floccul...

Embodiment 3

[0032] First, according to the Chinese patent application number 200910145058.4 "A kind of Trichomonad and its method of preparing melanin by liquid fermentation", the intracellular melanin is prepared by using the preservation number of CCTCC No: M 209193 Trichomonas YM-223: The bacterium block of Discobacteria YM-223 was inoculated in a 500mL Erlenmeyer flask filled with 250mL fermentation medium, and cultured at 26°C with constant temperature shaking at 150r / min for 10-15 days. After the cultivation, the fermentation broth is centrifuged to obtain mycelia. The obtained mycelium was dried at 55° C., ground, and the mycelium was added to a concentration of 2 mol / In L NaOH solution, leaching in 90°C water bath for 5h, suction filtration, the filtrate was adjusted to pH 2-3 with 12mol / L hydrochloric acid, and stood overnight, flocculent precipitates formed. After the flocculent precipitate was centrifuged at 5000r / min for 10min, deionized water was repeatedly added to the sep...

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Abstract

The invention discloses a lachnum melanin hair dye and a preparation method thereof. The preparation method is characterized in that: an agent A is prepared by dissolving para phenylene diamine, lachnum melanin, sodium sulfite, sodium bicarbonate, ascorbic acid, palmitic acid and ethylene diamine tetraacetic acid disodium in water and ammonia water to form an aqueous phase; adding into an oleic phase which is formed by heating to melt sodium carboxymethyl cellulose, nonylphenol polyoxyethylene ether and isopropanol or ethanol under stirring; and regulating the pH to be between 9.0 and 9.5 with the ammonia water; an agent B is prepared by adding the sodium carboxymethyl cellulose into water, aqueous solution of hydrogen peroxide and phenacetin, and regulating the pH to be between 3.4 and 4.0 by using phosphoric acid; and uniformly mixing the agent A with the agent B in the volume ratio of 1:(1-2) for use. By a hair-care dye with high safety, high efficiency and low toxicity provided bythe invention, the content of the para phenylene diamine in the hair dye is reduced, the antioxidation, the antiradiation, the light protectiveness and the safety of the lachnum melanin are exerted, and natural and lustrous dying effects can be kept.

Description

technical field [0001] The invention belongs to the technical field of hair dyes, and in particular relates to a hair dye of Trichodia granulosa melanin and a preparation method thereof. Background technique [0002] With the continuous development of society and the constant changes of the times, hair dye, as a hair cosmetic, has become a necessity for some people's daily life, and is valued by consumers and scientific researchers. [0003] According to "Journal of Hengyang Normal University" (2009, 30 (6): 85-88), existing natural hair dyes are much superior than chemical hair dyes in avoiding skin allergies and side effects; but natural hair dyes are also There are some problems: First, the stability of natural pigments is poor, mainly because natural pigments are easily affected by external factors such as pH value, light (especially ultraviolet light), temperature, etc., which will change the structure or composition of natural pigments , so that its color changes; the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K8/99A61Q5/10A61K8/19A61K8/22A61K8/23A61K8/34A61K8/36A61K8/41A61K8/44A61K8/67A61K8/73A61K8/86
Inventor 叶明汪燕王于顺
Owner HEFEI UNIV OF TECH
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