Phase change inks containing graphene-based carbon allotrope colorants, water-based ink and using method thereof
A carbon allotrope, phase change ink technology, applied in the direction of ink, copy/marking method, application, etc., can solve the problems of complex technology, pigment ink jetting, etc.
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Embodiment 1
[0188] Preparation of Pigment Dispersion Extrudate A. The curable amide gelling agent, the triamide resin, described in Example VIII of US Patent 7,279,587, was prepared in the form of flakes or blocks and then processed into powder using a blender. Thereafter, powdered triamide resin (38.1 equivalents) and carbon nanotubes (12.2 equivalents) were mixed for 30 minutes in a LITTLEFORD M5 mixer set at 0.8 amps. Subsequently, the powder mixture was fed into a DAVO counter-rotating twin-screw extruder (model VS 104, available from Deutsche Apparate-Vertrieborganisation GmbH & Co, Troisdorf, Germany) at a rate of 0.8 lbs / hr. The contents of the extruder were then mixed at 70°C at 50 RPM. The outlet temperature was set at 75°C. The extruded dispersion (extrudate A) was melt mixed with other ink ingredients to form an ink.
[0189] Ink Example 1. Extrudate A (1 equiv) and PETROLITE CA-11 (a dipolyurethane; 0.3 equiv) were weighed in a 250 mL beaker (A). will be purchased from Cr...
Embodiment 2
[0192] A carbon nanotube-based ink was prepared as in Ink Example 1, except that the double polyurethane WB-5 dispersant purchased from Baker Petrolite was used instead of PETROLITE CA-11.
Embodiment 3
[0194] A carbon nanotube-based ink was prepared as in Ink Example 1, except that the double polyurethane WB-17 dispersant purchased from Baker Petrolite was used instead of PETROLITE CA-11.
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