Photosensitive resin composition, photosensitive transfer material, partition wall and method for forming same, optical device and method for manufacturing same, and display
A technology of photosensitive resin and photosensitive resin layer, which is applied in the field of photosensitive resin composition and photosensitive transfer material, can solve the problems of deterioration of coating film formation, difficulty in uniform coating, difficulty in obtaining uniform film, etc., and achieve suppress splash effect
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Synthetic example 1
[0147] It can be synthesized through the two steps shown below.
[0148] : Synthesis of resin A1
[0149] Under a nitrogen flow, 15 g of methyl ethyl ketone (MEK) was added to a 300 ml three-neck flask provided with a cooling tube, and heated to 70° C. under a water bath. 12.5 g of 2-(perfluorooctyl)-ethyl acrylate (FAAC8, produced by Unimatec (Unimatec) Co., Ltd.) dissolved in 20 g of MEK was added dropwise thereto with a plunger pump for 2 hours, respectively. 0.024mol) and polyethylene oxide monomer (PE350, NOF Co., Ltd.) 12.5g (0.029mol) solution and 2,2'-azobis(isobutyric acid) bis A solution of 0.131 g (0.001 mol) of methyl ester (V601, manufactured by Wako Pure Chemical Industries, Ltd.). After completion of the dropwise addition, the mixture was stirred for 5 hours.
[0150] Through the above operations, 2-(perfluorooctyl)-ethyl acrylate (FAAC8) and polyethylene oxide monomer (PE350) were copolymerized to synthesize resin A1 with FAAC8 / PE350=50 / 50 (mass ratio).
[...
Synthetic example 2
[0157] It can be synthesized through the two steps shown below.
[0158] : Synthesis of Resin B1
[0159] Under a nitrogen flow, 15 g of methyl ethyl ketone (MEK) was added to a 300 ml three-neck flask provided with a cooling tube, and heated to 70° C. under a water bath. 12.5 g of 2-(perfluorooctyl)-ethyl acrylate (FAAC8, produced by Unimatec (Unimatec) Co., Ltd.) dissolved in 20 g of MEK was added dropwise thereto with a plunger pump for 2 hours, respectively. 0.024mol) and polyethylene oxide monomer (PE350, NOF Co., Ltd.) 12.5g (0.029mol) solution and 2,2'-azobis(isobutyric acid) bis A solution of 0.131 g (0.001 mol) of methyl ester (V601, manufactured by Wako Pure Chemical Industries, Ltd.). After completion of the dropwise addition, the mixture was stirred for 5 hours.
[0160] Through the above operations, 2-(perfluorooctyl)-ethyl acrylate (FAAC8) and polyethylene oxide monomer (PE350) were copolymerized to synthesize resin B1 with FAAC8 / PE350=50 / 50 (mass ratio).
[...
Synthetic example 3
[0167] It can be synthesized through the two steps shown below.
[0168] : Synthesis of resin C1
[0169] Under a nitrogen flow, 15 g of methyl ethyl ketone (MEK) was added to a 300 ml three-neck flask provided with a cooling tube, and heated to 70° C. under a water bath. 18.8 g of 2-(perfluorooctyl)-ethyl acrylate (FAAC8, produced by Unimatec (Unimatec) Co., Ltd.) dissolved in 20 g of MEK was added dropwise thereto with a plunger pump for 2 hours, respectively. 0.036mol) and polyethylene oxide monomer (PE350, NOF Co., Ltd.) 6.3g (0.015mol) solution and 2,2'-azobis(isobutyric acid) bis A solution of 0.118 g (0.001 mol) of methyl ester (V601, manufactured by Wako Pure Chemical Industries, Ltd.). After completion of the dropwise addition, the mixture was stirred for 5 hours.
[0170] Through the above operations, 2-(perfluorooctyl)-ethyl acrylate (FAAC8) and polyethylene oxide monomer (PE350) were copolymerized to synthesize resin C1 having FAAC8 / PE350=75 / 25 (mass ratio).
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