Silicon carbide granule enhancement type tin-silver-zinc compound solder and manufacture method thereof
A silicon carbide particle and enhanced technology, which is applied in welding equipment, welding/cutting media/materials, welding media, etc., can solve problems such as not being able to meet environmental protection, and achieve good mechanical properties, simple preparation methods, and long service life.
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Embodiment 1
[0026] The formula of the silicon carbide particle-reinforced tin-silver-zinc composite solder according to this embodiment is: tin-silver-zinc solder and 0.3% silicon carbide particles. The average size of silicon carbide particles is 10 μm, and in the tin-silver-zinc solder, the mass ratio of tin, silver, and zinc is 96.1:3:0.9.
[0027] The solder of this example is recorded as: 0.3% SiC reinforced Sn-3% Ag-0.9% Zn, and its preparation process is as follows:
[0028] ①. Heat the tin, silver and zinc with a purity of 99.99% to 1200°C in a vacuum melting furnace under the protection of argon according to the formula ratio, and at the same time add magnetic stirring to make the alloy composition uniform, then water-cool and solidify, and then melt the alloy After turning over, reheat to 1200°C to melt, and at the same time, add magnetic stirring and water cooling, repeat this at least five times, and obtain a button-shaped tin-silver-zinc solder with a diameter of 3.0 to 3.5 c...
Embodiment 2
[0031] The silicon carbide particle-reinforced tin-silver-zinc composite solder according to this embodiment includes tin-silver-zinc solder and 0.1% silicon carbide particles. The silicon carbide particles have an average size of 10 μm. The tin-silver-zinc solder is composed of tin, silver, zinc and indium in a mass ratio of 95:3.5:0.5:1.
[0032] The solder in this example is marked as: 0.1% SiC reinforced Sn-3.5% Ag-0.5% Zn-1% In, and its preparation process is as follows:
[0033] ①. The tin, silver, zinc and indium with a purity of 99.99% are heated to 1200°C in a vacuum melting furnace under the protection of argon according to the formula ratio, and magnetically stirred at the same time to make the alloy composition uniform, and then water-cooled and solidified. Turn the alloy over and reheat it to 1200°C to melt, and at the same time add magnetic stirring and water cooling, so repeat at least five times to get a button-shaped tin-silver-zinc solder with a diameter of ...
Embodiment 3
[0036] The silicon carbide particle-reinforced tin-silver-zinc composite solder according to this embodiment includes tin-silver-zinc solder and 0.5% silicon carbide particles. The silicon carbide particles have an average size of 10 μm. The tin-silver-zinc solder is composed of tin, silver, zinc and gallium with a purity of 99.99% in a mass ratio of 94.6:3.7:1.2:0.5.
[0037] The solder in this example is marked as: 0.5% SiC reinforced Sn-3.7% Ag-1.2% Zn-0.5% Ga, and its preparation process is as follows:
[0038] ①. The tin, silver, zinc and gallium with a purity of 99.99% are heated to 1200°C in a vacuum melting furnace under the protection of argon according to the formula ratio, and magnetically stirred at the same time to make the alloy composition uniform, and then water-cooled and solidified. Turn the alloy over and reheat it to 1200°C to melt, and at the same time add magnetic stirring and water cooling, so repeat at least five times to get a button-shaped tin-silver...
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