Polishing composition for semiconductor wafer, production method thereof, and polishing method
A semiconductor and composition technology, which is applied in the field of semiconductor wafer grinding compositions, and can solve the problems of inability to obtain grinding speed and surface roughness.
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[0076] Add 520kg JIS No. 3 sodium silicate (sada-silicate) (SiO 2 : 28.8% by weight, Na 2 O: 9.7% by weight, H 2 O: 61.5% by weight), uniformly mixed to prepare diluted sodium silicate with a silicon dioxide concentration of 4.5% by weight. This diluted sodium silicate was passed through a column of 1000 liters of H-type strongly acidic cation exchange resin (AMBERLITE IR120B produced by ORGANO Corporation) regenerated in advance with hydrochloric acid to carry out dealkalization to obtain 3800 kg of silica with a concentration of 3.7% by weight and a pH of 2.9 active silicic acid. In this active silicic acid, the content rates of Na and K per unit of silica were 80 ppm and 5 ppm, respectively. Next, rice uses the method of accumulation to make the colloidal particles grow. That is, to a part of 580 kg of the obtained active silicic acid, a 20% by weight tetramethylammonium hydroxide aqueous solution was added with stirring to adjust the pH to 8.7, and the mixture was kept...
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