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Method for detecting puff-by-puff stability of blueberry-flavored heated cigarettes by using nuclear magnetic resonance hydrogen spectrum

A technology of proton nuclear magnetic resonance spectrum and stability, which is applied in the direction of using nuclear magnetic resonance for analysis, etc., and can solve problems such as inability to accurately reflect mass fluctuations

Pending Publication Date: 2022-05-20
CHINA TOBACCO HENAN IND
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Problems solved by technology

[0004] The purpose of the present invention is to provide a method for detecting the puff-by-puff stability of blueberry-flavored heated cigarettes by proton nuclear magnetic resonance spectroscopy, so as to solve the subjective and one-sidedness of the artificial sensory evaluation method, which can only reflect some characteristics of flavors and fragrances, and cannot be accurate Problems reflecting fluctuations in its quality

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  • Method for detecting puff-by-puff stability of blueberry-flavored heated cigarettes by using nuclear magnetic resonance hydrogen spectrum
  • Method for detecting puff-by-puff stability of blueberry-flavored heated cigarettes by using nuclear magnetic resonance hydrogen spectrum

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[0026] The technical solution of the present application is described in detail below, and the following examples are only exemplary, and can only be used to explain and illustrate the technical solution of the present invention, and cannot be interpreted as a limitation to the technical solution of the present invention.

[0027] The invention provides a method for detecting the puff-by-puff stability of blueberry-flavored heated cigarettes by using hydrogen nuclear magnetic resonance spectrum. Taking blueberry-flavored heated cigarettes as the object, a rotary puff-by-puff smoking machine is used to smoke, collect the aerosol of each heated cigarette, solvent extraction and concentration, the obtained sample is dissolved with a deuterated reagent, and the nuclear magnetic hydrogen of the corresponding sample is obtained by nuclear magnetic resonance technology Spectrum, through the chemical shift, peak height, peak area and other information on the H NMR fingerprint spectrum,...

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Abstract

The invention relates to a method for detecting puff-by-puff stability of a blueberry-flavored heated cigarette by using a nuclear magnetic resonance hydrogen spectrum, which comprises the following steps of: smoking by using a rotary puff-by-puff smoking machine by taking the blueberry-flavored heated cigarette as an object, collecting aerosol of each puff of heated cigarette, extracting and concentrating by using a solvent, and detecting the puff-by-puff stability of the blueberry-flavored heated cigarette by using a deuterated reagent solvent. Nuclear magnetic hydrogen spectrums of corresponding samples are obtained through the nuclear magnetic resonance technology, and the similarity of spectrograms of all the samples is compared through information such as chemical shift, peak height and peak area on nuclear magnetic resonance hydrogen spectrum fingerprints, so that the puff-by-puff stability of the blueberry-flavored heated cigarettes is measured. The method is accurate and efficient, and is suitable for puff-by-puff stability analysis and detection of the blueberry-flavored heated cigarettes.

Description

technical field [0001] The invention relates to the field of detection of novel tobacco heated cigarettes, and more particularly relates to a method for detecting the puff-by-puff stability of blueberry-flavored heated cigarettes by using hydrogen nuclear magnetic resonance spectroscopy. Background technique [0002] In recent years, new types of tobacco have received widespread attention, among which heated cigarettes (HTP) are considered to be more acceptable to consumers because of their sensory experience closest to traditional cigarettes. Heated cigarettes have attracted many tobacco product consumers due to their advantages and characteristics such as less harmfulness, high safety, and better meeting the physical and psychological needs of smokers, showing a good momentum of development in the international market. [0003] Currently, there are various flavors of heated cigarettes, among which blueberry-flavored heated cigarettes are a product that appeared earlier and...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N24/08
CPCG01N24/08
Inventor 席高磊万帅陈芝飞于建春郑峰洋陈泽少杜佳李耀光蔡莉莉王清福刘前进赵旭马胜涛
Owner CHINA TOBACCO HENAN IND
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