Oil-control sunscreen makeup primer and preparation method thereof
The technology of makeup primer and caprylated chitosan is applied in cosmetic preparations, cosmetic preparations, cosmetics and other directions, and can solve the problem of affecting the makeup effect and makeup retention, adding a small amount, poor oil control effect, and pre-makeup. It can prevent excessive oil secretion, prolong the makeup effect, and prevent the makeup from dullness.
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Embodiment 1
[0036] An oil-control sunscreen makeup primer. The raw materials in parts by weight include: 8 parts of N-caprylylated chitosan modified kaolin, 8 parts of core-shell structure sunscreen particles, 12 parts of glycerin, 6 parts of squalane, 4 parts of iso Isononyl nonanoate, 2 parts hyaluronic acid, 0.8 parts octanoylglycine, 0.8 parts tocopherol, 0.2 parts ascorbic acid, 60 parts water.
[0037] Among them, the preparation method of N-octanoylated chitosan modified kaolin is: A) chitosan is dissolved in a mixed solvent of water, pyridine and tetrahydrofuran to obtain a chitosan solution, wherein the quality of chitosan and the mixed solvent The volume ratio is 1g:30mL, the volume ratio of water and pyridine tetrahydrofuran in the mixed solvent is 1:2:1; B) Add capryloyl chloride tetrahydrofuran solution dropwise to the chitosan solution under ice bath conditions, and heat up to 35°C Stir the reaction for 1.5h, the molar ratio of the octanoyl chloride in the tetrahydrofuran solut...
Embodiment 2
[0045] An oil-control sunscreen makeup primer. The raw materials in parts by weight include: 3 parts of N-caprylylated chitosan modified kaolin, 5 parts of core-shell structure sunscreen particles, 3 parts of caprylic acid / capric acid triglyceride, 1 part of angle Squalane, 3 parts isononyl isononanoate, 5 parts glycerin, 0.1 part ascorbic acid, 0.5 part tocopherol, 1 part hyaluronic acid, 30 parts water.
[0046] Among them, the preparation method of N-octanoylated chitosan modified kaolin is: A) chitosan is dissolved in a mixed solvent of water, pyridine and tetrahydrofuran to obtain a chitosan solution, wherein the quality of chitosan and the mixed solvent The volume ratio is 1g:20mL, and the volume ratio of water and pyridinetetrahydrofuran in the mixed solvent is 1:1:1; B) Add caprylyl chloride tetrahydrofuran solution dropwise to the chitosan solution under ice bath conditions, and heat up to 30°C Stir the reaction for 2h, the molar ratio of octanoyl chloride in the tetrahy...
Embodiment 3
[0054] An oil-control sunscreen makeup primer. The raw materials in parts by weight include: 5 parts of N-caprylylated chitosan modified kaolin, 8 parts of core-shell structure sunscreen particles, 7 parts of caprylic / capric triglyceride, and 3 parts of angle Squalane, 5 parts isononyl isononanoate, 8 parts glycerin, 0.5 part ascorbic acid, 1 part tocopherol, 0.5 part hyaluronic acid, 50 parts water.
[0055] Among them, the preparation method of N-octanoylated chitosan modified kaolin is: A) chitosan is dissolved in a mixed solvent of water, pyridine and tetrahydrofuran to obtain a chitosan solution, wherein the quality of chitosan and the mixed solvent The volume ratio is 1g:50mL, and the volume ratio of water and pyridine tetrahydrofuran in the mixed solvent is 1:1:1; B) Add octanoyl chloride tetrahydrofuran solution dropwise to the chitosan solution under ice bath conditions, and heat up to 40°C Stir the reaction for 1 hour, the molar ratio of octanoyl chloride in the tetrahy...
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