A method for the separation and detection of isomers in the racemate of Frelaner
A technology for fralana racemate and fralana racemate, which is applied in the field of separation and detection of isomers in fralana racemate, and achieves the effects of good separation effect and high sensitivity
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[0025] Unless otherwise defined, the technical terms used in the following embodiments have the same meaning as commonly understood by those skilled in the art to which the present invention belongs. The test reagents used in the following examples, unless otherwise specified, are conventional biochemical reagents; the experimental methods, unless otherwise specified, are conventional methods.
[0026] The present invention will be described in detail below in conjunction with the embodiments and accompanying drawings.
[0027] 1. Instruments and reagents
[0028] Instruments and reagents Model and specification factory High performance liquid chromatography LC-20AT,SPD-20A,SIL-20A SHIMADZU Electronic balance ES 225SM-DR Precisa chiral column AD-H (4.6mm×250mm, 5μm) Daicel Frelaner racemate 99.21% Medicin Biotechnology Co., Ltd. n-Hexane HPLC Tianjin Chuanpu Weiye Technology Co., Ltd. Isopropanol HPLC Xilong Sc...
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