Electrolytic nickel (ALLOY) plating solution
A technology of plating solution and electrolytic nickel, applied in circuits, printed circuits, electrical components, etc., can solve the problems of poor structure, insufficient filling, insufficient filling of electrolytic nickel plating solution, etc., to increase the amount of nickel precipitation, The effect of firm engagement
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Embodiment 1 to 6、 comparative example 1 to 3
[0163] A 12 mm square evaluation printed circuit board (manufactured by Japan Circuit Co., Ltd.) having a laser guide hole with an aspect ratio of 0.88 (φ45 μm×40 μmD) was used as a model of the minute concave portion.
[0164] The sectional view of the periphery 10 of the plated part is as figure 1 shown. After attaching a copper foil 13 with a thickness of 12 μm to the via hole forming part of the substrate 11 made of BT (Bismaleimide-Triazine) with a thickness of 0.4 mm, a prepreg type build-up resin 12 with a thickness of 60 μm is laminated, and then laser Make a blind hole (hereinafter sometimes referred to as "conducting hole" or "guide hole") 14 with a diameter of 45 μm and a depth of 40 μm, and conduct electroless copper plating on the outer surface of the substrate (the surface of the build-up resin 12 ) and the guide hole 14 A seed layer 15 of about 1 μm is formed on the inner wall surface of the .
[0165] Then it is formed by a dry film photoresist (DFR: Dry Film...
Embodiment 7 to 8、 comparative example 4
[0192] A copper wire (φ0.9mm) and a copper plate (20mm×20mm×0.3mmt) with a masked back surface were used as a model of the electronic component to be joined.
[0193] Such as image 3 As shown, prepare two copper plates 22 after shielding the back side by the masking material 22a, clamp the copper wire 21 with the unshielded surface of the two copper plates 22, and fix it with the auxiliary tool 23, and make the copper wire 21 and An electronic component sample 20 in which a minute gap 24 is formed between copper plates 22 .
[0194]
[0195] An electrolytic nickel plating solution was prepared by dissolving in deionized water so as to be 600 g / L of nickel sulfamate, 10 g / L of nickel chloride, and 30 g / L of boric acid, respectively.
[0196] The additives shown in Table 4 were added to the above-mentioned electrolytic nickel plating solution so as to be added in the amounts shown in Table 4, and dissolved.
[0197] Then, an appropriate amount of 100 g / L aqueous sulfamic ac...
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