Method and device for preparing sodium methoxide by coupling steam permeation and alkaline process
A technology of vapor permeation and sodium methoxide, which is applied in the preparation of metal alcohols, the separation/purification of hydroxyl compounds, organic chemistry, etc., can solve the problems of high energy consumption, high equipment investment cost, and low recovery rate of methanol, so as to save operating costs , Reduce energy consumption, simple and convenient operation
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[0020] The present invention provides a device for preparing sodium methoxide coupled by vapor permeation-alkali method. The device is mainly formed by coupling a sodium methoxide reaction module and a methanol dehydration module, and its structural diagram is shown in the attached figure 1 shown. The device comprises a sodium methoxide reactor 2, a pressurizing device 4 and a vapor permeation membrane separation device 5, wherein: the sodium methoxide reactor 2 is provided with a top liquid material inlet, a top gas material outlet, a bottom gas material inlet and a bottom liquid material outlet; The steam permeation membrane separation device 5 is provided with a raw material inlet, a retentate material outlet and a permeate material outlet; the top liquid material inlet of the sodium methoxide reactor 2 is provided with a raw material preheater 1; the bottom liquid material outlet is connected to the sodium methoxide product Cooler 3, its top gas material outlet is connecte...
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