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A kind of cosmetic containing pine pollen extract and its preparation process

A technology of pine pollen and extract, applied in the biological field, can solve the problems of unfeasible extraction of pine pollen flavonoids, inability to effectively precipitate by adding acid, and inability to solve problems through microporous membranes, achieving less impurities, less skin irritation, and compatibility Good results

Active Publication Date: 2020-04-21
烟台新时代健康产业日化有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Among the several flavonoid extraction processes at present, the hot water extraction method has more impurities and the yield is not high; the alkali extraction and acid precipitation method is not feasible for the extraction of pine pollen flavonoids, and it is found that adding acid cannot effectively precipitate it; High; the process of enzyme extraction and alcohol extraction is simple and easy, with high yield and less impurities, but after trying it, it is found that the system will continue to generate fine particles, and the microporous membrane cannot solve the problem.

Method used

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  • A kind of cosmetic containing pine pollen extract and its preparation process
  • A kind of cosmetic containing pine pollen extract and its preparation process
  • A kind of cosmetic containing pine pollen extract and its preparation process

Examples

Experimental program
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Effect test

Embodiment 1

[0028] A cosmetic containing pine pollen extract, its components include: 52% water, 5% glycerol, 5% 1,3-butanediol, 1% nicotinamide, 5% pine pollen extract , 3% stearyl alcohol, 5% D-panthenol, 5% caprylic capric triglyceride, 5% synthetic squalane, 2% silicone oil 200, 3% jojoba oil, 1% PMX-0345 silicone oil, 1% Phenoxyethanol, 4% Tween-60 and 3% NIKKOL Nikkomulese SE.

[0029] Wherein, the preparation technology of described pine pollen extract, steps are as follows:

[0030] (1) Alcohol extraction: take pine pollen, add ethanol with a concentration of 75wt%, extract in a reflux water bath at 85° C. for 3 hours, and extract twice to obtain an extract; wherein, the weight ratio of ethanol to pine pollen is 20:1;

[0031] (2) Filtration and concentration: the extract of step (1) is filtered while it is hot, and the obtained filtrate is concentrated under reduced pressure at 45°C until the liquid is in the form of an extract;

[0032] (3) Alcohol precipitation: cool the conc...

Embodiment 2

[0038] A cosmetic containing pine pollen extract, its components include: 57% water, 3% glycerol, 3% 1,3-butanediol, 2% nicotinamide, 4% pine pollen extract in terms of weight percentage , 5% stearyl alcohol, 3% D-panthenol, 6% caprylic capric triglyceride, 3% synthetic squalane, 1% silicone oil 200, 1% jojoba oil, 2% PMX-0345 silicone oil, 1% Phenoxyethanol, 6% Tween-60 and 3% NIKKOL Nikkomulese SE.

[0039] Wherein, the preparation technology of described pine pollen extract, steps are as follows:

[0040] (1) Alcohol extraction: take pine pollen, add ethanol with a concentration of 75wt%, 40W, 40KHz, 45°C ultrasonic-assisted reflux extraction for 2 hours, and obtain an extract; wherein, the weight ratio of ethanol to pine pollen is 30:1;

[0041] (2) Filtration and concentration: the extract of step (1) is filtered while it is hot, and the obtained filtrate is concentrated under reduced pressure at 60°C until the liquid is in the form of an extract;

[0042] (3) Alcohol p...

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Abstract

The invention belongs to the field of biotechnology, in particular to a cosmetic containing pine pollen extract and a preparation process thereof. The present invention adopts the method of ethanol extraction and ethanol alcohol precipitation to extract pine pollen, solves the problem that fine precipitation is formed in the pine pollen extract, obtains stable pine pollen extract; The present invention uses suitable macroporous adsorption resin to carry out flavonoids Refining and purification; the concentrate is prepared with polyol aqueous solution to form pine pollen extract with polyol aqueous solution as the system. The obtained extract is stable, has good compatibility with cosmetics, and has little irritation to the skin. It is suitable for the application of pine pollen extract to The field of cosmetics provides the basis. The pine pollen extraction method adopted in the present invention has simple process, high yield, less impurities, strong operability, the obtained pine pollen extract has good stability, no precipitation, low risk of allergies, and good compatibility with cosmetic substrates. The obtained cosmetic has the effects of whitening, anti-aging, antibacterial and anti-inflammation.

Description

technical field [0001] The invention belongs to the field of biotechnology, in particular to a cosmetic containing pine pollen extract and a preparation process thereof. Background technique [0002] Since ancient times, pine pollen has been a treasure of food therapy and beauty treatment. Its application in skin care products has a long history. It is recorded in "Materia Medica Congxin" in the Qing Dynasty that "it is good for all kinds of acne and sores, and it is wet and rotten without scabs". Modern scientific research shows that pine pollen contains a variety of vitamins, proteins, amino acids, fats and other nutrients, known as "super miniature nutrition bank". Active ingredients such as pollen flavonoids have whitening, anti-aging, antibacterial and anti-inflammatory effects, and are often used in cosmetics. [0003] Among the several flavonoid extraction processes at present, the hot water extraction method has more impurities and the yield is not high; the alkali ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K8/9761A61Q19/00A61Q19/02A61Q19/08A61Q17/00A61P29/00A61P31/02A61P31/04
CPCA61K8/9761A61K2800/10A61K2800/805A61K2800/82A61P29/00A61P31/02A61P31/04A61Q17/005A61Q19/00A61Q19/02A61Q19/08
Inventor 牟维林邹鹏飞于建伟陶宇赵乐荣隋海松魏星唐文金
Owner 烟台新时代健康产业日化有限公司
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