A kind of plant composite sunscreen and its preparation and application
A technology of sunscreen and plant, applied in the direction of cosmetic preparations, toiletry preparations, skin care preparations, etc., can solve the problems that have not been seen in the application of sunscreen, achieve good sunscreen effect, inhibit activity, and scavenge free radicals Effect
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Embodiment 1
[0027] A kind of preparation method of plant composite sunscreen
[0028] Ashitaba roots were dried and crushed, added with 70% volume concentration of ethanol solution, ultrasonically assisted for 1 h, filtered and concentrated under reduced pressure, then absorbed by AB-8 macroporous resin and eluted with organic solvents, and concentrated under reduced pressure to obtain Ashitaba Extract.
[0029] Dried and crushed Rosa roxburghii fruit, added 80% volume concentration of ethanol solution, ultrasonically assisted extraction for 1 h, filtered and concentrated under reduced pressure, then absorbed by AB-8 macroporous resin and eluted with organic solvent, and concentrated under reduced pressure to obtain Rosa roxburghii Extract.
[0030] Dry and crush the mangosteen peel, add 80% volume concentration of ethanol solution, ultrasonically treat for 30 min, extract overnight, filter and concentrate under reduced pressure, redissolve the extract with water, extract with ethyl acet...
Embodiment 2
[0033] UV absorption test of plant compound sunscreen: prepare sunscreen base, add the prepared plant compound sunscreen into the sunscreen base at a ratio of 10%, and measure the SPF value and PA value of the plant compound sunscreen by SPF-290S critical wavelength.
[0034] The specific formula of sunscreen is as follows (w / %): stearic acid 6.0, glycerin 6.0, cetyl alcohol 4.0, octyl palmitate 3.0, glyceryl stearate 2.0, lanolin 2.0, polyethylene glycol (40) stearic acid Ester 1.0, Dimethicone 1.0, Lauramidopropyl Dimethylamine 2.0, Olive Oil 2.0, Acrylic Copolymer 0.5, Triethanolamine 1.5, Plant Complex Sunscreen 10, Deionized Water 59.
[0035] With 3M adhesive tape as a support, the sample is pressed at 1mg / cm 2 Spread it evenly on the tape, and use the sunscreen matrix without plant compound sunscreen as a blank control to measure the SPF value and PA critical wavelength of the plant compound sunscreen. The experimental results are shown in Table 1.
[0036] Table 1 UV...
Embodiment 3
[0040] Antioxidant ability test of plant compound sunscreen:
[0041] 1), FRAP method - total antioxidant capacity test
[0042] Principle: The principle of FRAP method to measure total antioxidant capacity is that antioxidants can reduce Ferric-tripyridyltrizaine (Fe3+ -TPTZ) produces blue Fe 2+ -TPTZ, followed by absorbance measurement of blue Fe 2+ -TPTZ to obtain the total antioxidant capacity of the sample.
[0043] Test method: Dissolve the plant compound sunscreen in DMSO to make a 1mM solution, react with FRAP reagent under acidic conditions for 30 minutes, then measure its absorbance at 597 nm, and use 1mM Vc as a positive control. The experimental results are shown in Table 2.
[0044] Table 2 FRAP method—total antioxidant capacity test
[0045] sample FRAP value 1 mM Vc 1.59 4:2:4 6.72 3:3:4 6.56
[0046] As can be seen from Table 2, the plant composite sunscreen prepared by the present invention has very good total antioxidant cap...
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