Device and method for liquid trace sampling based on air thermal expansion
A micro-sampling and air-heating technology, which is applied to the analysis of materials and instruments, can solve problems such as difficulty in ensuring the consistency of analysis results, deviation of personal perspective, complex structure, etc., and achieve simple structure, consistency assurance, and good compatibility Effect
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[0036] This embodiment is based on the liquid micro-sampling method of thermal expansion of air, comprising the following steps:
[0037] 1. Use an electronic balance to measure the mass of the surface acoustic wave sensor, denoted as m 1 , and then embed the sensor in the bottom of sampling cup 1.
[0038] 2. Use the syringe 5 to extract the sample liquid to be tested, turn the sampling cup 1 upside down, use the syringe 5 to inject 1ml of the sample liquid into the sample cavity 31 of the sampling cup with a volume of 1.5ml, pull out the syringe 5, and place the sampling cup 1 upright ;
[0039]3. Place the sampling cup 1 in the detection chamber 6, insert it on the sensor detection base 63, control the mechanical telescopic arm 62 to wrap the heating plate 61 around the sampling cup 1, and control the heating temperature of the heating plate 61 to rise from 25°C to 37°C °C, as the air pressure expands, the liquid in the sample chamber 31 flows out; the volume V of the sam...
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