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A kind of pretreatment method of purple sweet potato pigment extract

A technology of purple sweet potato pigment and extract, which is applied to chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problems of long time consumption, poor stability of natural pigments, and easy oxidation, etc., to improve clarification effect and clarification effect Significant, corrosion-reducing effect

Active Publication Date: 2015-12-02
QINGDAO PENGYUAN KANGHUA NATURAL PROD
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  • Summary
  • Abstract
  • Description
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AI Technical Summary

Problems solved by technology

[0004] (1) The method of multi-stage natural sedimentation is time-consuming, low in production efficiency, and the stability of natural pigments is poor and easy to be oxidized, which will lead to a certain loss of pigments
[0005] (2) The method of filtration is adopted, the operation time is short, but the treatment is not thorough. Some macromolecular substances in the solution such as starch, protein and cellulose will aggregate with time, and precipitate slowly, which will be absorbed by the subsequent column. operation causing blockage

Method used

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Embodiment Construction

[0014] The specific production steps of the present invention are described in detail below in conjunction with the technical solutions:

[0015] (1) Pigment extraction: Wash the purple sweet potato tuber, slice and shred, weigh 200g, add 300mL 2% (mass to volume ratio, w / v%) calcium chloride aqueous solution according to the material-to-liquid ratio of 1:1.5, and then add Concentrated hydrochloric acid or concentrated sulfuric acid, the pH of the final extract is 2.0, intermittent stirring and extraction for 4 hours, and gauze filtration to obtain the extract.

[0016] (2) Mixing and sedimentation: Tannic acid needs to be formulated into a solution first, and then added, so as to ensure uniform mixing, otherwise if the solid powder of tannic acid is added, the dispersion will be uneven, and the local concentration will be too thick, and local flaky precipitation will easily occur; Tannic acid must be deionized water. The presence of metal ions in the aqueous solution can easily pr...

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PUM

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Abstract

The invention belongs to the technical field of food processing, and relates to a pretreatment method of a purple sweet potato pigment extract solution. The preparation method comprises the following preparation processes: cleaning a purple sweet potato root tuber, cutting into slices and then cutting into shreds; adding 1.0-2.5% of (mass-to-volume ratio, w / v%) calcium chloride water solution to soak and extract; adjusting the pH value of the extract solution to 1.5-2.5; soaking and extracting for 2-6 hours; filtering or centrifuging the extract solution, and then adding a tannic acid aqueous solution while controlling the adding amount of tannic acid being 0.02-0.03% (mass-to-volume ratio, w / v%); evenly mixing and standing for 2-4 hours; separating and removing solid sediments, so as to obtain clear and stable pigment extract solution. The method has the characteristics that the light transmittance of the extract solution at 660nm can be improved by 6-10 times by adopting the composite adding precipitation method of calcium chloride and tannic acid; the clarification effect is significant; the dosage of concentrated hydrochloric acid or concentrated sulfuric acid for adjusting the pH value can be reduced by over 20% by adding calcium chloride in extraction. Therefore, corrosion on equipment caused by acid is also reduced.

Description

Technical field [0001] The invention relates to a pretreatment method for a purple sweet potato pigment extract, which belongs to the technical field of food processing, in particular adding calcium chloride when extracting pigments to reduce the precipitation of starch impurities and reduce the amount of acid used for pH adjustment; After finishing, add tannic acid, combine with protein, polysaccharide and calcium ion in the solution, play a role of co-precipitation, remove impurities that easily cause precipitation, and obtain a clear and stable solution to facilitate subsequent resin adsorption and purification operations of the pigment solution . Background technique [0002] Purple sweet potato pigment is a natural product extracted from the root tuber of Ipomoea batatas (Ipomoea batatas). The main component is cornflower 3-glucoside anthocyanin. As a kind of natural food coloring, purple sweet potato pigment is not only safe and non-toxic, but also has high nutritional val...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B61/00C09B67/54
Inventor 常秀莲赵镇雷徐菡
Owner QINGDAO PENGYUAN KANGHUA NATURAL PROD
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