A kind of preparation method of heat insulation and anti-fog film layer for automobile glass
A technology for automobile glass and anti-fog film, which is applied in the field of preparation of heat-insulating and anti-fog film layers for automobile glass, can solve the problems of poor anti-fog function durability, incomplete anti-fog effect, etc., and achieves the effect of eliminating the generation of fog.
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Embodiment 1
[0022] 1. Preparation of heat insulating resin;
[0023] Add 20g 1-propylene glycol methyl ether acetate-2 ester, 12g TDI aromatic isocyanate in 50g ethyl acetate, stir at room temperature for 2h, then add 5g10nm mesoporous silica and 0.2g polyether alkyl siloxane leveling agent, Stir at room temperature for 1 hour to obtain a heat-insulating resin.
[0024] 2. Preparation of anti-fog film layer;
[0025] First, degrease the glass surface with methanol, then perform physical polishing, and then clean it with tap water and distilled water respectively, and then dry it for later use.
[0026] Use thermal insulation resin system to coat the surface of clean and dry automotive glass. The coating process is spraying. Immediately after the coating is completed, spray the surface with transparent nano-silver solution, and then place it at room temperature for leveling. After leveling, put the glass film on Place at 100°C for 1 hour.
[0027] Fogging occurred at the beginning of th...
Embodiment 2
[0029] 1. Preparation of heat insulating resin;
[0030] Add 20g 1-propylene glycol methyl ether acetate-2 ester, 12g TDI aromatic isocyanate to 50g ethyl acetate, stir at room temperature for 2h, then add 5g10nm mesoporous silica and 0.2g and 10g transparent nano-silver solution polyether alkyl silicon Oxane leveling agent, stir at room temperature for 1h.
[0031] 2. Preparation of anti-fog film layer;
[0032] First, degrease the glass surface with methanol, then perform physical polishing, and then clean it with tap water and distilled water respectively, and then dry it for later use.
[0033] Stir 1 g of N-(2-aminoethyl)-3-aminopropylmethyldimethoxysilane and 49 g of water at room temperature for 1 h, then add ethanol, and continue stirring for 10 min to obtain a coupling agent solution. Wipe the prepared coupling agent solvent on the dry and clean glass surface, and then place it at 100°C for 1h.
[0034] After the surface of the automobile glass treated by the coupl...
Embodiment 3
[0037] 1. Preparation of heat insulating resin;
[0038] Add the aromatic isocyanate of 20g hydroxyl-containing acrylate A450 (Bayer company) and 12g TDI in 50g ethyl acetate, stir at room temperature for 2h, then add 7g20nm silicon dioxide and 0.2g polyether alkyl siloxane leveling agent, stir at room temperature 1h, the heat insulating resin is obtained.
[0039] 2. Preparation of anti-fog film layer;
[0040] First, degrease the glass surface with methanol, then perform physical polishing, and then clean it with tap water and distilled water respectively, and then dry it for later use.
[0041] Use thermal insulation resin system to coat the surface of clean and dry automotive glass. The coating process is spraying. Immediately after the coating is completed, spray the surface with transparent nano-silver solution, and then place it at room temperature for leveling. After leveling, put the glass film on Place at 100°C for 1 hour.
[0042] Fogging occurred at the beginnin...
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