Method for preparing molybdenum electrode rod by die forging method
A molybdenum electrode and die forging technology, applied in the field of material preparation, can solve the problems of shrinkage cavities, surface cracks, increased wire drawing burrs, etc., and achieve the effects of uniform quality, regular rod size, and no surface cracks.
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Embodiment 1
[0020] The first step, the selection of molybdenum powder
[0021] The selected particle size is 3.2μm, and the loose ratio is 1.05g / cm 3 Molybdenum powder is used as raw material for die forging.
[0022] The second step is to press the billet
[0023] Put the molybdenum powder selected in the first step into a cylindrical mold, then put the molybdenum powder loaded mold into a cold isostatic press for pressing, and set the pressure of the cold isostatic press to 180Mpa for pressing. After pressing, hold the pressure for 8 minutes to obtain a molybdenum billet with a diameter of 55 mm;
[0024] The third step, sintering molybdenum billet
[0025] Put the two kinds of molybdenum rods prepared in the second step into the intermediate frequency furnace, fill the furnace with hydrogen, and then carry out segmental sintering. First, heat for 3 hours so that the furnace temperature rises from 20°C to 1000°C, and then keep it warm 1.5 hours; heat for 1.5 hours to 1250°C, hold fo...
Embodiment 2
[0030] The first step, the selection of molybdenum powder
[0031] The selected particle size is 3.9μm, and the loose ratio is 1.2g / cm 3 Molybdenum powder is used as raw material for die forging.
[0032] The second step is to press the billet
[0033] Put the molybdenum powder selected in the first step into a cylindrical mold, then put the molybdenum powder loaded mold into a cold isostatic press for pressing, and set the pressure of the cold isostatic press to 200Mpa for pressing. After pressing, hold the pressure for 15 minutes to obtain a molybdenum billet with a diameter of 90 mm;
[0034] The third step, sintering molybdenum billet
[0035] Put the two kinds of molybdenum rods prepared in the second step into the intermediate frequency furnace, fill the furnace with hydrogen, and then carry out segmental sintering. First, heat for 4 hours so that the furnace temperature rises from 20°C to 1000°C, and then keep it warm 2.5 hours; heat for 1.5 hours to 1250°C, hold fo...
Embodiment 3
[0040] The first step, the selection of molybdenum powder
[0041] The selected particle size is 3.5μm, and the loose ratio is 1.12g / cm 3 Molybdenum powder is used as raw material for die forging.
[0042] The second step is to press the billet
[0043] Put the molybdenum powder selected in the first step into a cylindrical mold, then put the molybdenum powder loaded mold into a cold isostatic press for pressing, and set the pressure of the cold isostatic press to 190Mpa for pressing. After pressing, hold the pressure for 10 minutes to obtain a molybdenum billet with a diameter of 120 mm;
[0044] The third step, sintering molybdenum billet
[0045] Put the two kinds of molybdenum rods prepared in the second step into the intermediate frequency furnace, fill the furnace with hydrogen, and then carry out segmental sintering. First, heat for 4 hours so that the furnace temperature rises from 20°C to 1000°C, and then keep it warm 2.5 hours; heat for 1.5 hours to 1250°C, hold ...
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