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Method for extracting lavender extract with tank-type ultrasonic machine

A technology of lavender extract and lavender, which is applied in the field of ultrasonic extraction of lavender extract, can solve the problems of low extraction rate, non-continuous production, and unrealization, and achieve the effects of improving content and quality, highlighting technological progress, and reducing impurity content

Inactive Publication Date: 2013-06-19
郑刚 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

In addition to the volatile lavender essential oil, lavender, an aromatic plant, also contains a large amount of plant waxes, proteins, glycosides, sugars and other components that are extremely beneficial to the human body but are not volatile. It cannot be extracted and utilized; (2) CO 2 The extraction rate of lavender extract obtained by supercritical extraction method is ≤5.6%, and the final extraction temperature is ≥50°C. The extraction rate of this extraction method is low, and the active ingredients of lavender extract are easily destroyed when the temperature is above 50°C; (3 ) The extraction rate of lavender extract by fixed bed extraction is ≤2.9%. This method cannot be produced continuously, the recovery rate of organic solvent is low, and the production process is in a non-closed state, which will have a certain impact on the environment.
[0003] The lavender extract obtained by this method, in addition to volatile lavender essential oil, also contains a large amount of non-volatile plant waxes, proteins, glycosides, sugars and other components, accounting for 20-25% of the total amount of the extract, and effective The use of high-value components cannot be achieved through traditional extraction methods, which is where the value of this method lies.

Method used

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  • Method for extracting lavender extract with tank-type ultrasonic machine

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Embodiment

[0021] Raw material disposal: pick high-quality, non-rotten fresh lavender stems, leaves, and petals, put them in the shade under natural conditions, and then use them after crushing. The water content of the crushed materials is ≤ 20%, and the crushed particle size is ≤ 40 mesh;

[0022] Preparation scheme 1: Take 10kg of lavender that has been crushed through a 20-mesh sieve, and put it into the organic solvent ethanol (95%) produced by Xinjiang Jiepule Biotechnology Co., Ltd. at a mass ratio of 1:8, which meets the national standard JB / T 20126-2009 In the tank-type ultrasonic extraction machine, keep the temperature of the ultrasonic extraction tank at 40°C for 35 minutes to obtain the lavender ethanol mixture; input the mixture into the extraction liquid slag and squeeze the separation device, separate the slag and the extraction mixture, and input the extraction mixture into In the dynamic cycle low-temperature decompression (-0.08MPa) evaporator concentrator, keep the tem...

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Abstract

The invention provides a method for extracting a lavender extract with a tank-type ultrasonic machine, picking stems, leaves and petals of fresh lavender, drying in the shade, and pulverizing to 10-40 meshes; mixing the pulverized lavender and an organic solvent in a mass ratio of 1:(5-10), and extracting in a tank-type ultrasonic extraction machine at 25-50 DEG C for 20-40 minutes to obtain a lavender-organic solvent mixture; putting the lavender-organic solvent mixture in a liquid-residue press separator, separating the residues, and carrying out press separation at 20-100 kg / h to obtain a lavender extract-organic solvent mixture; and putting the lavender extract-organic solvent mixture in a dynamic loop low-temperature evaporation concentrator, reducing the pressure to -0.08 MPa, and recovering the organic solvent at 20-40 DEG C to obtain the lavender extract, wherein the yield of the lavender extract is at least 12%.

Description

technical field [0001] The invention relates to the extract of lavender, and is especially suitable for a method for ultrasonically extracting the lavender extract, which can effectively improve the recovery rate compared with the prior art. Background technique [0002] Traditional lavender extraction methods: (1) Steam distillation to obtain a single lavender essential oil whose main components are volatile aromatic esters and aromatic alcohols. The extraction rate of lavender essential oil is ≤0.9%. In addition to the volatile lavender essential oil, lavender, an aromatic plant, also contains a large amount of plant waxes, proteins, glycosides, sugars and other components that are extremely beneficial to the human body but are not volatile. It cannot be extracted and utilized; (2) CO 2 The extraction rate of lavender extract obtained by supercritical extraction is ≤5.6%, and the final extraction temperature is ≥50°C. The extraction rate of this extraction method is low...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
Inventor 王余彪郑刚
Owner 郑刚
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