Process for preparing pulp by using salix mongolia by chemical mechanical method
A technology of chemical machinery and Salix salix, which is applied in textiles, papermaking, and fiber raw material processing to achieve the effects of reducing dosage, improving performance, and increasing flexibility
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Embodiment 1
[0037] Three-year-old Salix wood chips are pulped in the following steps after the first stage of steaming and squeezing:
[0038] 1. Cellulase pretreatment, the pretreatment conditions are: temperature 60-65℃, time 1.5h, pH value 5-6, enzyme dosage 20IU / g absolute dry pulp, pulp concentration 10%;
[0039] 2. Carry out the first stage chemical pre-impregnation of the slurry treated in the above step 1 with sodium alkali hydrogen peroxide solution. Relative to the mass of the absolute dry pulp, the amount of chemical components in the dipping solution and the process conditions are: NaOH 3.0% , H 2 O 2 3.0%, MgSO 4 0.2%, EDTA 0.2%, immersion temperature 60-70℃, liquid ratio 1:4;
[0040] 3. The slurry impregnated in step 2 is subjected to the second stage of extrusion and decompression, the extrusion temperature is 60-70°C, and the decompression volume ratio is 6:1;
[0041] 4. Carry out the second stage of enzymatic pretreatment of the squeezed and decomposed slurry in step 3. The ...
Embodiment 2
[0049] Three-year-old Salix wood chips are pulped in the following steps after the first stage of steaming and squeezing:
[0050] 1. Cellulase pretreatment, the pretreatment conditions are: temperature 60-65℃, time 1.5h, pH value 5-6, enzyme dosage 40IU / g absolute dry pulp, pulp concentration 10%, the enzyme used is solid cellulase ;
[0051] 2. Carry out the first stage chemical pre-impregnation of the slurry treated in the above step 1 with sodium alkali hydrogen peroxide solution. Relative to the mass of the absolute dry pulp, the amount of chemical components in the dipping solution and the process conditions are: NaOH 4.4% , H 2 O 2 4.0%, MgSO 4 0.2%, EDTA 0.2%, immersion temperature 60-70℃, liquid ratio 1:4;
[0052] 3. The slurry impregnated in step 2 is subjected to the second stage of extrusion and decompression, the extrusion temperature is 45-60℃, and the decompression volume ratio is 4:1;
[0053] 4. Carry out the second stage of enzymatic pretreatment of the squeezed ...
Embodiment 3
[0061] Three-year-old Salix wood chips are pulped in the following steps after the first stage of steaming and squeezing:
[0062] 1. Cellulase pretreatment, the pretreatment conditions are: temperature 60-65℃, time 1.5h, pH value 5-6, enzyme dosage 30IU / g absolute dry pulp, pulp concentration 10%, the enzyme used is solid cellulase ;
[0063] 2. Carry out the first stage chemical pre-impregnation of the slurry treated in the above step 1 with sodium alkali hydrogen peroxide solution. Relative to the mass of the absolute dry pulp, the amount of chemical components in the dipping solution and the process conditions are: NaOH 3.7% , H 2 O 2 3.5%, MgSO 4 0.2%, EDTA 0.2%, immersion temperature 60-70℃, liquid ratio 1:4;
[0064] 3. The slurry impregnated in step 2 is subjected to the second stage of extrusion and decompression, the extrusion temperature is 55-65°C, and the decompression volume ratio is 5:1;
[0065] 4. Carry out the second stage of enzymatic pretreatment of the squeezed...
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