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Process for preparing pulp by using salix mongolia by chemical mechanical method

A technology of chemical machinery and Salix salix, which is applied in textiles, papermaking, and fiber raw material processing to achieve the effects of reducing dosage, improving performance, and increasing flexibility

Inactive Publication Date: 2012-02-08
QILU UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In order to improve the mechanical pulping performance of salix salix and improve the whiteness and strength performance index of pulp, the present invention provides a kind of salix chemical pulp with good whiteness and strength performance The mechanical pulping process fundamentally solves the problems of low pulp whiteness, poor strength performance and low pulp yield caused by the short and small fibers of Salix salix

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] Three-year-old Salix wood chips are pulped in the following steps after the first stage of steaming and squeezing:

[0038] 1. Cellulase pretreatment, the pretreatment conditions are: temperature 60-65℃, time 1.5h, pH value 5-6, enzyme dosage 20IU / g absolute dry pulp, pulp concentration 10%;

[0039] 2. Carry out the first stage chemical pre-impregnation of the slurry treated in the above step 1 with sodium alkali hydrogen peroxide solution. Relative to the mass of the absolute dry pulp, the amount of chemical components in the dipping solution and the process conditions are: NaOH 3.0% , H 2 O 2 3.0%, MgSO 4 0.2%, EDTA 0.2%, immersion temperature 60-70℃, liquid ratio 1:4;

[0040] 3. The slurry impregnated in step 2 is subjected to the second stage of extrusion and decompression, the extrusion temperature is 60-70°C, and the decompression volume ratio is 6:1;

[0041] 4. Carry out the second stage of enzymatic pretreatment of the squeezed and decomposed slurry in step 3. The ...

Embodiment 2

[0049] Three-year-old Salix wood chips are pulped in the following steps after the first stage of steaming and squeezing:

[0050] 1. Cellulase pretreatment, the pretreatment conditions are: temperature 60-65℃, time 1.5h, pH value 5-6, enzyme dosage 40IU / g absolute dry pulp, pulp concentration 10%, the enzyme used is solid cellulase ;

[0051] 2. Carry out the first stage chemical pre-impregnation of the slurry treated in the above step 1 with sodium alkali hydrogen peroxide solution. Relative to the mass of the absolute dry pulp, the amount of chemical components in the dipping solution and the process conditions are: NaOH 4.4% , H 2 O 2 4.0%, MgSO 4 0.2%, EDTA 0.2%, immersion temperature 60-70℃, liquid ratio 1:4;

[0052] 3. The slurry impregnated in step 2 is subjected to the second stage of extrusion and decompression, the extrusion temperature is 45-60℃, and the decompression volume ratio is 4:1;

[0053] 4. Carry out the second stage of enzymatic pretreatment of the squeezed ...

Embodiment 3

[0061] Three-year-old Salix wood chips are pulped in the following steps after the first stage of steaming and squeezing:

[0062] 1. Cellulase pretreatment, the pretreatment conditions are: temperature 60-65℃, time 1.5h, pH value 5-6, enzyme dosage 30IU / g absolute dry pulp, pulp concentration 10%, the enzyme used is solid cellulase ;

[0063] 2. Carry out the first stage chemical pre-impregnation of the slurry treated in the above step 1 with sodium alkali hydrogen peroxide solution. Relative to the mass of the absolute dry pulp, the amount of chemical components in the dipping solution and the process conditions are: NaOH 3.7% , H 2 O 2 3.5%, MgSO 4 0.2%, EDTA 0.2%, immersion temperature 60-70℃, liquid ratio 1:4;

[0064] 3. The slurry impregnated in step 2 is subjected to the second stage of extrusion and decompression, the extrusion temperature is 55-65°C, and the decompression volume ratio is 5:1;

[0065] 4. Carry out the second stage of enzymatic pretreatment of the squeezed...

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Abstract

The invention relates to a process for preparing pulp by performing enzyme pretreatment on salix mongolia by a chemical mechanical method in the field of processes for preparing the pulp by chemical mechanical methods, which solves the problems of low whiteness, low intensity properties and low yield of paper pulp due to the shortness of salix mongolia fibers. The process comprises the following steps of: performing a first stage of cellulose enzyme pretreatment on salix mongolia pulp which is subjected to a first stage of extrusion defibering after steaming; soaking the pulp which is subjected to the enzyme pretreatment by using soda hydrogen dioxide solution; performing a second stage of extrusion defibering after the soaking; performing a second stage of dextranase pretreatment on the pulp which is subjected to the extrusion defibering; performing a second stage of soaking on the pulp which is subjected to the enzyme pretreatment by using the soda hydrogen dioxide solution; performing a first stage of defibrination and high-concentration storage bleaching on the soaked pulp together with impregnation liquid; and performing a second stage of defibrination to produce chemical mechanical pulp with high whiteness, high yield and high strength. By the process, the mechanical pulping performance of fast growing shrub salix mongolia can be improved, the application range of high-yield pulp of the salix mongolia can be widened, and the application value of the salix mongolia can be improved.

Description

technical field [0001] The invention relates to a chemical-mechanical pulping process, in particular to a chemical-mechanical pulping process of salixase pretreatment. Background technique [0002] The pulp and paper industry has always occupied an important position in the global industrial manufacturing industry. The production and consumption level of paper and cardboard has become an important symbol to measure a country's economic development level and social progress. With the development of the economy, the consumption of paper products shows a continuous growth trend. Compared with the rising market demand, the raw material gap of China's paper industry is very large. China is short of timber resources, and the output of timber used for papermaking is far from meeting the needs of the development of the papermaking industry. Coupled with the shortcomings in the scale and quality of domestic waste paper recycling, the shortage of papermaking raw materials has become...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D21C5/00
Inventor 杨桂花陈嘉川孔凡功王守娟
Owner QILU UNIV OF TECH
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