Application of extractive and effective parts of datura flower in preparing medication for anti tumor
A technology of anti-tumor drugs and effective parts, which is applied in the field of traditional Chinese medicine and can solve problems such as pharmacological research that does not describe therapeutic activity
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Embodiment 1
[0057] Take 1 kg of Dajinhua, add 95% ethanol to reflux and extract for 2 hours each time, extract 3 times, combine the extracts, and evaporate the solvent to obtain 90 grams of Dajinhua extract.
Embodiment 2
[0059] Take 500 grams of Dajinhua, add 5 liters of petroleum ether, reflux and extract 3 times, each time for 1 hour, combine the extracts and concentrate to 50 milliliters to obtain the crude extract of Dajinhua oil, add 75 grams of activated carbon to the crude extract , stirred for 30 minutes, filtered and washed the activated carbon with ethyl acetate for 5 times, combined the filtrate and ethyl acetate washings, and evaporated the solvent to obtain refined datura oil.
Embodiment 3
[0061] 500 grams of datura flowers were extracted with CO2 supercritical, the extraction temperature was 35°C, the extraction pressure was 12Mpa, and the CO2 flow rate was 2.5kg / hr. After extraction in the separation tank for 240 minutes, the pressure of the separation tank was 8Mpa and the temperature was 40°C. The extract was placed in volatile oil In the separator, let it stand and centrifuge to obtain 4.6 grams of datura oil.
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