Oil-based drilling fluid shear-lifting agent composition, oil-based drilling fluid shear-lifting agent product and preparation method thereof, and oil-based drilling fluid
A technology of oil-based drilling fluid and cutting agent, applied in the field of oil-based drilling fluid, can solve the problems of difficulty in opening the pump, sticking of the drilling fluid to the drill pipe, affecting the rheology of the system, etc., so as to ensure that the wellbore is clean and has strong temperature resistance , the effect of good application prospects
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preparation example Construction
[0064] In the preparation method of the present invention, acrylic acid, acrylamide and 2-acrylamidotetradecanesulfonic acid have undergone a three-way copolymerization reaction, so the surface grafting of the composite modified hectorite of the present invention has acrylic acid, acrylamide and 2- Random copolymer of acrylamidotetradecanesulfonic acid. Preferably, in the composite modified hectorite, the structural unit from acrylic acid monomer: the structural unit from acrylamide monomer: the molar ratio of the structural unit from 2-acrylamidotetradecanesulfonic acid monomer is 3-10: 0.5-5: 0.5-3, more preferably 4-8: 1-3: 0.5-2; more preferably 5-7: 1-2: 1-1.5.
[0065] In the present invention, based on the weight of the composite modified hectorite, the structural unit derived from acrylic acid monomer, the structural unit derived from acrylamide monomer and the structural unit derived from 2-acrylamidotetradecanesulfonic acid monomer The proportion of the total weight o...
preparation example 1A
[0129] (1) Add 0.06 mol of 1,12-dibromododecane, 0.084 mol of 1,4-dimethylpiperazine and 75 mL of dimethyl sulfoxide into a 1000 mL dry three-necked flask, and react at 55°C for 3 hour, then add N-methylimidazole 0.002mol and N-methylmorpholine 0.002mol, react at 55° C. for 3 hours, and remove the solvent by distillation under reduced pressure to obtain polyquaternium salt;
[0130] (2) In a 100mL dry three-necked flask, add 0.01mol of 1,3,5-tris(4-naphthyloxy-1,8-dioic acid)phthalic anhydride and 25mL of m-cresol in sequence, Stir under low temperature, when 1,3,5-tris(4-naphthyloxy-1,8-dioic acid) phthalic anhydride is completely dissolved, add 0.005mol of 3,3'-diaminobenzidine, stir at room temperature After 45 minutes, heat to 75°C, react for 4 hours, then react at 180°C for 10 hours, after the reaction, cool to room temperature, and quickly pour it into 2000mL of methanol to obtain a large amount of solid precipitation, then wash the solid precipitate repeatedly with meth...
preparation example 2A
[0133] (1) Add 0.1 mol of 1,12-dibromododecane, 0.092 mol of 1,4-dimethylpiperazine and 85 mL of dimethyl sulfoxide into a 1000 mL dry three-necked flask, and react at 45°C for 6 Hour, add N-methylimidazole 0.0022mol and N-methylmorpholine 0.0022mol again, react at 45 ℃ for 6 hours, after decompression distillation removes solvent, make polyquaternium salt;
[0134] (2) In a 100mL dry three-necked flask, add 0.015mol of 1,3,5-tris(4-naphthyloxy-1,8-dioic acid) phthalic anhydride and 28mL of m-cresol in turn, under nitrogen protection Under stirring, when 1,3,5-tris(4-naphthyloxy-1,8-dioic acid)phthalic anhydride is completely dissolved, add 0.006mol of 3,3'-diaminobenzidine, and stir at room temperature After 50 minutes, heat to 78°C, react for 3 hours, and then react at 185°C for 8 hours. After the reaction, cool to room temperature, and quickly pour it into 2000mL of methanol to obtain a large amount of solid precipitation, and then wash the solid with methanol repeatedly P...
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