Solid soil improvement agent containing titanium citrate and potassium citrate and application thereof
A technology of soil improver and potassium citrate, which is applied in application, soil conditioning materials, organic fertilizers, etc., can solve the problems of unsatisfactory effect, high cost, complicated process, etc., and achieve the reduction of soil compaction hardness, easy control, and raw materials simple effect
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Embodiment 1
[0019] In the embodiment of the present invention, a solid soil conditioner containing titanium citrate and potassium citrate consists of the following raw materials in parts by weight: 9 parts of titanium citrate, 22 parts of potassium citrate, 25 parts of black rice husk, 11 parts of heartwood, 5 parts of N-methylpyrrolidone.
[0020] Mix N-methylpyrrolidone with 12 times the mass of deionized water to prepare N-methylpyrrolidone solution. The black rice husk and split wood were mixed and crushed, passed through a 120-mesh sieve, and an aqueous solution of acetic acid 4 times the mass of the two was added, and stirred at 88°C for 2.5 hours to obtain a mixture. Mix potassium citrate and N-methylpyrrolidone solution, raise the temperature to 80°C, and stir at this temperature for 55 minutes, then add titanium citrate, raise the temperature to 160°C, heat up to 160°C, and heat it under a hydrogen atmosphere for 2 hours, then lower the temperature to 72 ℃, add the mixture, and ...
Embodiment 2
[0022] In the embodiment of the present invention, a solid soil conditioner containing titanium citrate and potassium citrate is composed of the following raw materials in parts by weight: 17 parts of titanium citrate, 30 parts of potassium citrate, 35 parts of black rice husk, 19 parts of heartwood, 12 parts of N-methylpyrrolidone.
[0023] Mix N-methylpyrrolidone with 12 times the mass of deionized water to prepare N-methylpyrrolidone solution. Black rice husks and split wood were mixed and crushed, passed through a 120-mesh sieve, an aqueous acetic acid solution 4 times the mass of the two was added, and stirred at 88°C for 2.8 hours to obtain a mixture. Mix potassium citrate and N-methylpyrrolidone solution, heat up to 80°C, and stir at this temperature for 60 minutes, then add titanium citrate, heat up to 160°C, heat up to 160°C, heat up to 2h in a hydrogen atmosphere, and then cool down to 72 ℃, add the mixture, and ultrasonically treat at this temperature for 40min, th...
Embodiment 3
[0025] In the embodiment of the present invention, a solid soil conditioner containing titanium citrate and potassium citrate consists of the following raw materials in parts by weight: 11 parts of titanium citrate, 24 parts of potassium citrate, 28 parts of black rice husk, 13 parts of heartwood, 7 parts of N-methylpyrrolidone.
[0026] Mix N-methylpyrrolidone with 12 times the mass of deionized water to prepare N-methylpyrrolidone solution. The black rice husk and split wood were mixed and crushed, passed through a 120-mesh sieve, and an aqueous solution of acetic acid 4 times the mass of the two was added, and stirred at 88°C for 2.6 hours to obtain a mixture. Mix potassium citrate and N-methylpyrrolidone solution, raise the temperature to 80°C, and stir at this temperature for 58 minutes, then add titanium citrate, raise the temperature to 160°C, heat up to 160°C, and heat up to 80°C for 2 hours, then cool down to 72 ℃, add the mixture, and ultrasonically treat at this te...
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