Method for preparing tobacco dendrobium candidum flavor with sorghum liquor as extraction solvent
A technique for extracting solvent from Dendrobium candidum, which is applied in the field of preparation of Dendrobium candidum spices for cigarettes, can solve problems such as insufficient permeability, and achieve the effect of improving aroma quality, transparency, and good coordination
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Embodiment 1
[0023] Take 50 grams of Dendrobium candidum, 5 grams of lovage, 15 grams of lychee core, and 15 grams of dried tomato, soak in 255 g of compound enzyme solution at 40°C for 3 hours, filter with suction, and remove the filtrate to obtain a compound of Dendrobium candidum. Add 255ml of sorghum wine (58 degrees) to the Dendrobium officinale compound, reflux in an 80v water bath for 4 hours, and filter to obtain the sorghum wine extract. Add 95% ethanol twice the mass to the sorghum liquor extract for alcohol precipitation, leave it at 4°C for 24 hours, and then concentrate it in a vacuum until the density is 1.08-1.15g / cm 3 . Add 30% of its mass of 1,2-propanediol and 20% of absolute ethanol to the concentrate, and mix evenly to obtain the Dendrobium candidum fragrance for smoking.
Embodiment 2
[0025] Take 50 grams of Dendrobium candidum, 5 grams of lovage, 15 grams of lychee core, and 15 grams of dried tomato, soak in 255 g of compound enzyme solution at 40°C for 3 hours, filter with suction, and remove the filtrate to obtain a compound of Dendrobium candidum. Add 255ml of sorghum wine (45°C) to the Dendrobium officinale compound, reflux in a water bath at 80°C for 4 hours, and filter to obtain the sorghum wine extract. Add 1 times the mass of 95% ethanol to the sorghum wine extract for alcohol precipitation, leave it at 4°C for 24 hours, and then concentrate it in a vacuum until the density is 1.08-1.15g / cm 3 . Add 30% of its mass of 1,2-propanediol and 20% of absolute ethanol to the concentrate, and mix evenly to obtain the Dendrobium candidum fragrance for smoking.
Embodiment 3
[0027] Take 50 grams of Dendrobium candidum, 5 grams of lovage, 15 grams of litchi core, and 15 grams of dried tomato, soak in 255 g of compound enzyme solution at 45°C for 3 hours, filter with suction, and remove the filtrate to obtain a compound of Dendrobium candidum. Add 340ml of sorghum wine (58°C) to the Dendrobium officinale compound, reflux in a water bath at 80°C for 4 hours, and filter to obtain the sorghum wine extract. Add 95% ethanol twice the mass to the sorghum liquor extract for alcohol precipitation, leave it at 4°C for 24 hours, and then concentrate it in a vacuum until the density is 1.08-1.15g / cm 3 . Add 30% of its mass of 1,2-propanediol and 20% of absolute ethanol to the concentrate, and mix evenly to obtain the Dendrobium candidum fragrance for smoking.
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