A kind of alkali-resistant disperse blue dye, its compound mixture and preparation method thereof
A technology of disperse dyes and disperse blue, applied in azo dyes, organic dyes, monoazo dyes, etc., can solve the problems of high pollution of dyeing waste liquid, non-compliance with energy saving and emission reduction, high cost, and reduce energy consumption and pollution. , The effect of excellent fastness and high improvement
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Embodiment 1
[0021] Add 44g of concentrated sulfuric acid with a mass concentration of 90-98% in the reaction three-necked flask, add 13g of 3-amino-5 nitrobenzisothiazole under stirring, maintain the temperature at 45-50°C, and keep it warm for 1.0 hour to make 3-amino-5 nitro Dissolve all the benzisothiazole until clear; add ice to cool down to 24°C, start adding 21.5g of nitrosylsulfuric acid dropwise, and use ice during the dropwise addition to ensure that the temperature of the material in the reactor remains at 15-20°C; take 1.5-2.0 hours After adding nitrosyl sulfuric acid, keep warm for another 3 hours, and the temperature is still controlled at 15-20°C; before the end of the diazonium reaction, do an end point test; after the test is passed, it will be a diazonium solution, ready to discharge.
[0022] While waiting for the diazo insulation reaction, use a 1000mL three-necked bottle for coupling, and prepare emulsifier OP-10 into a solution with a mass concentration of 10% for late...
Embodiment 2
[0025] Add 40 g of concentrated sulfuric acid with a mass concentration of 90-98% in the reaction three-necked flask, add 10 g of 3-amino-5 nitrobenzisothiazole under stirring, maintain the temperature at 45-50 ° C, and keep it warm for 1.0 hour to make 3-amino-5 nitro All benzisothiazole was dissolved until clear. Add ice to cool down to 24°C, start to add 20 g of nitrosyl sulfuric acid dropwise, and use ice to ensure that the temperature of the material in the reactor is maintained at 10-15°C during the dropwise addition. It takes 1.5-2.0 hours to finish adding nitrosyl sulfuric acid, and then keep it warm for 5 hours, and the temperature is still controlled at 10-15°C. Before the end of the diazonium reaction, do the end point detection. After passing the test, it is diazo liquid, ready to discharge.
[0026] While waiting for the diazo insulation reaction, use a 1000mL three-necked bottle for coupling, and prepare emulsifier OP-10 into a solution with a mass concentratio...
Embodiment 3
[0029] Add 50 g of concentrated sulfuric acid with a mass concentration of 90-98% in the reaction three-necked flask, add 15 g of 3-amino-5 nitrobenzisothiazole under stirring, maintain the temperature at 45-50 ° C, and keep it warm for 1 hour to make 3-amino-5 nitro All benzisothiazole was dissolved until clear. Add ice to cool down to 24°C, and start to add 25 g of nitrosylsulfuric acid dropwise. It takes 1.5-2.0 hours to finish adding the nitrosyl sulfuric acid, and then keep the temperature for 4 hours, and the temperature is still controlled at 15-20°C. Before the end of the diazonium reaction, do the end point detection. After passing the test, it is diazo liquid, ready to discharge.
[0030]While waiting for the diazo insulation reaction, use a 1000mL three-necked bottle for coupling, and prepare emulsifier OP-10 into a solution with a mass concentration of 10% for later use. Add 240g of water, 10g of emulsifier OP-10 solution with a mass concentration of 10%, and 0....
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