A kind of preparation method of antibacterial and anti-electromagnetic radiation composite film
A technology of anti-electromagnetic radiation and composite film, which is applied in the field of anti-electromagnetic radiation materials, can solve the problems of boron thermal neutron absorption performance decline, neutron shielding effect, large concrete volume, etc., and achieve high tensile strength and long-lasting shielding performance , The effect of simple preparation process
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example 1
[0017] First weigh 30g of cornstarch, put it into an oven, and dry it at 80°C for 5h, put the dried cornstarch into a 1L three-necked flask, and add 50g of polyvinyl chloride and 500mL of Put distilled water in a water bath, set it at 90°C and stir for 5 hours. After the reaction, lower the temperature to 60°C, then add 40mL of 5% citric acid solution and 20mL of pyridine into the flask, and stir for 1h to complete the activation. After cooling to room temperature; add acetone solution to the activated solution at a volume ratio of 1:1.5, stir and mix evenly, and add 10% of the total mass of dioctyl phthalate to the mixed solution as a plasticizer, and continue to magnetically Stir for 30 minutes, after stirring, the film liquid is obtained, and set aside; weigh 10g of sodium alginate powder in a 500mL reaction kettle, add 250mL of distilled water into the reaction kettle, set the temperature in the kettle to 60°C, and let it stand for 2h to make the sodium alginate Fully swel...
example 2
[0020] First weigh 40g of cornstarch, put it in an oven, and dry it at 90°C for 5.5h. Put the dried cornstarch into a 1L three-necked flask, and add 65g of polyvinyl chloride and 550mL of Put distilled water into a water bath, set it at 93°C and stir for 5.5 hours. After the reaction, lower the temperature to 65°C, then add 45mL of 5% citric acid solution and 25mL of pyridine into the flask, stir and activate for 1.5h After activation, cool to room temperature; add acetone solution to the activated solution at a volume ratio of 1:1.5, magnetically stir and mix evenly, and add a total mass of 13% dioctyl phthalate to the mixed solution as a plasticizer , continue magnetic stirring for 35 minutes, and obtain a membrane liquid after stirring, and set aside; weigh 13g of sodium alginate powder in a 500mL reaction kettle, add 275mL of distilled water to the reaction kettle, set the temperature in the kettle to 65°C, and let it stand for 3h to make The sodium alginate is fully swoll...
example 3
[0023]First, weigh 50g of cornstarch, put it in an oven, and dry it at 100°C for 6 hours. Put the dried cornstarch into a 1L three-necked flask, and add 80g of polyvinyl chloride and 600mL of Put distilled water in a water bath, set it at 95°C and stir for 6 hours. After the reaction, lower the temperature to 70°C, then add 50mL of 5% citric acid solution and 30mL of pyridine into the flask, stir and activate for 2h, and the activation is complete. After cooling to room temperature; add acetone solution to the activated solution at a volume ratio of 1:1.5, magnetically stir and mix evenly, and add 15% of the total mass of dioctyl phthalate to the mixed solution as a plasticizer, and continue to magnetically Stir for 40 minutes, after stirring, the film liquid is obtained, and set aside; weigh 15g of sodium alginate powder into a 500mL reaction kettle, add 300mL of distilled water to the reaction kettle, set the temperature in the kettle to 70°C, and let it stand for 4h to make ...
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