A kind of production method for preparing special fertilizer for potassium dihydrogen phosphate by-product shepherd's purse
A technology of potassium dihydrogen phosphate and production method, applied in chemical instruments and methods, applications, phosphorus compounds, etc., can solve the problems of wasting natural resources and polluting the environment, reducing the purity and loss of potassium dihydrogen phosphate products, and reducing production. cost, make up the cost of impurity removal, and reduce the production cost
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Embodiment 1
[0045] A production method for preparing potassium dihydrogen phosphate byproduct shepherd's purse special fertilizer, comprising the following steps:
[0046] (1) Preparation and mixing of raw materials: put phosphoric acid and carbonamide in a stirred reactor at a molar ratio of 1.4:1, raise the temperature to 120°C at a heating rate of 15°C / min, and control the stirring speed of the stirring tank to 200r / min to stir Mixed reaction 5h, obtain intermediate slurry;
[0047] (2) Preparation of KH 2 PO 4 : Add the alkaline potassium salt of 1.5mol 4h at a uniform speed into the reaction kettle containing the intermediate slurry obtained in step 1), and adopt a stirring speed of 200r / min stirring reaction for 60min to obtain the material containing nitrogen, phosphorus and potassium pulp;
[0048] (3) Cyclic crystallization filtration: the slurry obtained in step 2) containing nitrogen, phosphorus, and potassium is placed in a cooling crystallizer to cool to a temperature of 2...
Embodiment 2
[0054] A production method for preparing potassium dihydrogen phosphate byproduct shepherd's purse special fertilizer, comprising the following steps:
[0055] (1) Preparation and mixing of raw materials: put phosphoric acid and carbonamide in a stirred reactor at a molar ratio of 1.8:1, raise the temperature to 100°C at a heating rate of 15°C / min, and control the stirring speed of the stirring tank to 180r / min to stir Mixed reaction 4h, obtain intermediate slurry;
[0056] (2) Preparation of KH 2 PO 4 : Add the alkaline potassium salt of 1.4mol 3h at a uniform speed into the reaction kettle containing the intermediate slurry obtained in step 1), and adopt a stirring speed of 160r / min stirring reaction for 40min to obtain the material containing nitrogen, phosphorus and potassium pulp;
[0057] (3) Cyclic crystallization filtration: the slurry containing nitrogen, phosphorus, and potassium obtained in step 2) is placed in a cooling crystallizer to cool down to a temperature...
Embodiment 3
[0063] A production method for preparing potassium dihydrogen phosphate byproduct shepherd's purse special fertilizer, comprising the following steps:
[0064] (1) Preparation and mixing of raw materials: put phosphoric acid and carbonamide in a stirred reactor at a molar ratio of 1.5:1, raise the temperature to 105°C at a heating rate of 15°C / min, and control the stirring speed of the stirring tank to 190r / min to stir Mixed reaction 4.2h, obtain intermediate slurry;
[0065] (2) Preparation of KH 2 PO 4 : the alkaline potassium salt 3.3h of 1.45mol is added in the reaction kettle containing the intermediate slurry that step 1) makes at a uniform speed again, and adopting stirring speed is 180r / min stirring reaction 50min, obtains nitrogen, phosphorus, potassium slurry;
[0066] (3) Cyclic crystallization filtration: the slurry containing nitrogen, phosphorus, and potassium obtained in step 2) is placed in a cooling crystallizer to cool down to a temperature of 18° C., and ...
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