A kind of photocatalyst and its preparation method for removing condensed water trace steam turbine oil
A photocatalyst and turbine oil technology, which is applied in chemical instruments and methods, organic compound/hydride/coordination complex catalysts, physical/chemical process catalysts, etc., can solve the conditions of low load rate and photocatalytic degradation that are difficult to achieve , There is no such problem as an ideal material, and the effect of high load rate, low density and small grain size is achieved
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Embodiment 1
[0034] A photocatalyst for removing trace amounts of steam turbine oil, consisting of the following components:
[0035]
[0036]
[0037] The preparation method of the coating of Example 1 is:
[0038] (1) Put 1kg of 8nm nano TiO 2 The powder was added to 4kg of deionized water and dispersed by ultrasonic for 0.5h to obtain nano-TiO with good dispersion 2 ;
[0039] (2) Add polyethylene glycol to the concentrated slurry, stir and disperse for 1 hour, and cool to room temperature;
[0040] (3) After cooling, add 0.5kg of toluene diisocyanate and stir at a certain temperature for 0.5h at a high speed to obtain a prepolymer;
[0041] (4) Add ethylene glycol, glycerol and polysiloxane to the prepolymer, and continue to stir for 0.25 hours;
[0042] (5) The mixture prepared in (4) is heated and kept for 12 hours for curing to obtain.
[0043] The photocatalyst of Example 1 was analyzed by SEM image of TiO 2 The particles are filled in the pores of the foam to ensure nano-TiO 2 The photocataly...
Embodiment 2
[0045] A photocatalyst for removing trace amounts of steam turbine oil, consisting of the following components:
[0046]
[0047]
[0048] The preparation method of the coating of Example 2 is:
[0049] (1) Put 15kg of 8nm nano TiO 2 The powder was added to 60kg of deionized water, and ultrasonically dispersed for 0.8h to obtain nano-TiO with good dispersion 2 ;
[0050] (2) Add polyethylene glycol to the concentrated slurry, stir and disperse for 1 hour, and cool to room temperature;
[0051] (3) After cooling, add 30kg of toluene diisocyanate, stir at a high speed for 0.8h at a certain temperature to obtain a prepolymer;
[0052] (4) Add ethylene glycol, glycerol and polysiloxane to the prepolymer, and continue to stir for 0.5h;
[0053] (5) The mixture prepared in (4) is heated and kept for 12 hours for curing to obtain.
[0054] The catalytic efficiency of the photocatalyst of Example 2 is above 90%, the number of repetitions is more than three times, and the catalytic efficiency is a...
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