Method for ultrasonic extraction and separation of 10-deacetyl baccatin III from yew branch leaves
A technology of yew branches and leaves and acetyl baccatine, which is applied in the field of ultrasonic extraction and separation of 10-deacetyl baccatine III, can solve the problems of large solvent consumption and long soaking time, and achieves time saving, high speed and convenience. The effect of industrial production
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment Construction
[0026] Materials used in the test: short branches of European yew (air-dried, water content 5%-10%)
[0027] D101-1 macroporous adsorption resin
[0028] Case 1
[0029] Take 1Kg of dried European yew branches and leaves, crush them, add 10L of 0.1% (w / w) citric acid aqueous solution, put them into an ultrasonic instrument, and perform ultrasonication for 2 hours. Filter out 8L of dark yellow extract, detect by HPLC, contain 1.02g of 10-deacetylbaccatin III. Then add 10L of 0.1% (w / w) citric acid aqueous solution to the leaves, sonicate for 2 hours, and filter out 10L The left and right extracts were detected by HPLC. The second extract contained 0.21 g of 10-deacetylbaccatin III. Added 10 L of 0.1% (w / w) citric acid aqueous solution to the extracted leaves, and ultrasonicated for 2 Hour, obtain about 10L light yellow extract again, detect with HPLC, contain 10-deacetylbaccatin III in the extract for the third time and be 0.08g.
[0030] Case 2
[0031] Get 150Kg of dried ...
PUM
Property | Measurement | Unit |
---|---|---|
water content | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com