A kind of organic compound containing xanthene and its application on oled device
An organic compound, xanthene technology, applied in the field of OLED applications, the field of compound materials containing xanthene structure as the central skeleton, can solve problems such as different
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Embodiment 1
[0072] Embodiment 1: the synthesis of compound 6:
[0073] synthetic route:
[0074]
[0075] In a 250ml three-neck flask, under the protection of nitrogen, add 0.01mol raw material A1, 0.012mol raw material B1, 0.03mol sodium tert-butoxide, 5×10 -5 molpd 2 (dba) 3 , 5×10 -5 mol of tri-tert-butylphosphine, 150ml of toluene, heated to reflux for 24 hours, sampling point plate, the reaction was complete; natural cooling, filtration, rotary evaporation of the filtrate, column chromatography to obtain the target product, HPLC purity 99.4%, yield 71.5%;
[0076] Elemental analysis structure (molecular formula C 53 h 36 N 2 o 2 ): theoretical value C, 86.86; H, 4.95; N, 3.82; 0, 4.37; test value: C, 86.87;
[0077] HPLC-MS: The molecular weight of the material is 732.87, and the measured molecular weight is 733.14.
Embodiment 2
[0078] Embodiment 2: the synthesis of compound 3:
[0079] synthetic route:
[0080]
[0081] In a 250ml three-neck flask, under the protection of nitrogen, add 0.01mol raw material A1, 0.012mol raw material B2, 0.03mol sodium tert-butoxide, 5×10 -5 mol pd 2 (dba) 3 , 5×10 -5 mol of tri-tert-butylphosphine, 150ml of toluene, heated to reflux for 24 hours, sampling point plate, the reaction was complete; natural cooling, filtration, rotary evaporation of the filtrate, column chromatography to obtain the target product, HPLC purity 99.1%, yield 72.5%;
[0082] Elemental analysis structure (molecular formula C 56 h 40 N 2 O): theoretical value C, 88.86; H, 5.33; N, 3.70; O, 2.11; tested value: C, 88.87; H, 5.32; N, 3.71;
[0083] HPLC-MS: The molecular weight of the material is 756.93, and the measured molecular weight is 757.31.
Embodiment 3
[0084] Embodiment 3: the synthesis of compound 10:
[0085] synthetic route:
[0086]
[0087] In a 250ml three-neck flask, under the protection of nitrogen, add 0.01mol raw material A1, 0.012mol raw material C1, 0.03mol sodium tert-butoxide, 5×10 -5 mol pd 2 (dba) 3 , 5×10 -5 mol of tri-tert-butylphosphine, 150ml of toluene, heated to reflux for 24 hours, sampling point plate, the reaction was complete; natural cooling, filtration, filtrate rotary evaporation, column chromatography to obtain the target product, HPLC purity 99.5%, yield 71.8%;
[0088] Elemental analysis structure (molecular formula C 58 h 40 N 2 o 2 ): theoretical value C, 87.41; H, 5.06; N, 3.52; O, 4.02; test value: C, 87.43;
[0089] HPLC-MS: The molecular weight of the material is 796.95, and the measured molecular weight is 797.38.
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