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Zirconium mullite boron nitride carbon side sealing plate and manufacturing method

A zirconium-mullite and manufacturing method technology, applied in the field of zirconium-mullite boron nitride carbon side seal plate and manufacturing, can solve the problems of high equipment requirements and high manufacturing costs, and achieve good wear resistance, good bonding and The effect of abrasion resistance

Inactive Publication Date: 2018-11-20
阳谷信民耐火材料有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method also has relatively high requirements on equipment, and the manufacturing cost is relatively high.

Method used

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  • Zirconium mullite boron nitride carbon side sealing plate and manufacturing method

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A zirconium mullite boron nitride carbon side seal plate, which is composed of the following components (mass ratio): 10% zirconium mullite, 72% hexagonal boron nitride, 15% elemental boron powder, 3% graphite, carbon fiber ( Addition) 0.3%, thermosetting phenolic resin (addition) 20%.

[0033] Step 1) Premix hexagonal boron nitride, graphite, carbon fiber and some zircon mullite fine powder according to the above ratio to obtain powder A; put the additives in the carbon binder and stir evenly to obtain a composite binder B;

[0034] Step 2) Put the remaining zircon mullite in a high-speed mixer at a speed of 100 rpm, and add composite binder B, stir and mix evenly, then add powder A to fully mix to obtain a mixed uniform material, After the material is trapped for 24 hours, it is formed by vacuum pressure at room temperature, and the vacuum forming pressure is 300MPa;

[0035] Step 3) The molded product is cured at 200°C, fired at 1200°C for 10 hours, then impregnate...

Embodiment 2

[0037] A zirconium mullite boron nitride carbon side sealing plate, which is composed of the following components (mass ratio): 20% zirconium mullite, 67% hexagonal boron nitride, 10% elemental boron powder, 3% graphite, carbon fiber ( Addition) 0.3%, thermosetting phenolic resin (addition) 15%.

[0038] The manufacturing method of the above-mentioned zirconium mullite boron nitride carbon side sealing plate:

[0039] Step 1) Premix hexagonal boron nitride, graphite, carbon fiber and some zircon mullite fine powder according to the above ratio to obtain powder A; put the additives in the carbon binder and stir evenly to obtain a composite binder B;

[0040] Step 2) Put the remaining zircon mullite in a high-speed mixer at a speed of 100 rpm, and add composite binder B, stir and mix evenly, then add powder A to fully mix to obtain a mixed uniform material, After the material is trapped for 24 hours, it is formed by vacuum pressure at room temperature, and the vacuum forming p...

Embodiment 3

[0043] A zirconium mullite boron nitride carbon side seal plate, which is composed of the following components (mass ratio): 30% zirconium mullite, 62% hexagonal boron nitride, 5% elemental boron powder, 3% graphite, carbon fiber ( Addition) 0.3%, thermosetting phenolic resin (addition) 12%.

[0044] The manufacturing method of the above-mentioned zirconium mullite boron nitride carbon side sealing plate:

[0045] Step 1) Premix hexagonal boron nitride, graphite, carbon fiber and some zircon mullite fine powder according to the above ratio to obtain powder A; put the additives in the carbon binder and stir evenly to obtain a composite binder B;

[0046] Step 2) Put the remaining zircon mullite in a high-speed mixer at a speed of 100 rpm, and add composite binder B, stir and mix evenly, then add powder A to fully mix to obtain a mixed uniform material, After the material is trapped for 24 hours, it is formed by vacuum pressure at room temperature, and the vacuum forming press...

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PUM

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Abstract

The invention discloses a zirconium mullite boron nitride carbon side sealing plate which comprises the following components (in percentage by mass): 5-30% of zirconium mullite, 10-80% of hexagonal boron nitride, 1-20% of an additive, 0.5-5% of graphite, 0.1-5% of an (external) carbon fiber and 5-20% of a carbon binding agent (external). A manufacturing method of the zirconium mullite boron nitride carbon side sealing plate comprises the following steps: premixing the hexagonal boron nitride, the graphite, the carbon fiber and a part of the zirconium mullite so as to obtain powder A, uniformlystirring monomer boron with the carbon binding agent so as to obtain a composite binding agent B; putting the zirconium mullite of different granules into a mixing machine, adding the composite binding agent B, uniformly stirring and mixing, sufficiently mixing with the powder A so as to obtain a uniform mixed material, ageing the mixture, and carrying out normal-temperature molding; carrying outhigh-temperature carbonization, soaking treatment and annealing, and further carrying out grinding on a grinding machine, thereby obtaining a double-roller thin cast side sealing plate. The zirconiummullite boron nitride carbon side sealing plate disclosed by the invention has the characteristics of being low in friction coefficient, high in strength, good in wearing resistance, good in thermalshock resistance, good in corrosion resistance, small in investment equipment, low in cost, and the like.

Description

technical field [0001] The invention belongs to the field of inorganic non-metallic materials and high-temperature engineering refractory ceramics, and relates to a zirconium mullite boron nitride carbon side sealing plate and a manufacturing method. Background technique [0002] Pair-roll thin strip continuous casting is a near-net shape continuous casting. Thin strip continuous casting consists of two water-cooled rolls rotating in opposite directions and a pair of side sealing plates to form a molten pool or crystallizer. Use the submerged nozzle to inject molten steel into the molten pool through the flow distributor. The molten steel solidifies on the surface of the water-cooled roll. The gap between is squeezed out. Side sealing process and side sealing plate are one of the core technologies of thin strip continuous casting. The thin strip continuous casting process requires the ceramic refractory material of the side sealing plate to have excellent comprehensive pr...

Claims

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Application Information

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IPC IPC(8): C04B35/583C04B35/622C04B35/626C04B41/83
CPCC04B35/583C04B35/622C04B35/62605C04B41/4823C04B41/83C04B2235/3463C04B2235/421C04B2235/425C04B2235/5248C04B2235/77C04B2235/96
Inventor 田守信申娟娟张兆路田守民王新建蒲锡鹏田伟杰
Owner 阳谷信民耐火材料有限公司
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